benzo(1,2-c:3,4-c')bis(1,2,5)oxadiazole-1,6-dioxide

Base Information

• Chemical Name: benzo(1,2-c:3,4-c')bis(1,2,5)oxadiazole-1,6-dioxide
• CAS No.: 5714-12-5
• Molecular Formula: C6H2N4O4
• Molecular Weight: 194.1045
• Mol file: 5714-12-5.mol

Synonyms:Benzo[1,2-c,3,4-c']bis[1,2,5]oxadiazol-1,6-dioxid;Benzo<1.2-c><3.4-c>difuroxan;benzo[1,2-c,3,4-c']bis-[1,2,5]oxadiazole-1,6-dioxide;4,5-Furoxano-benzofuran (asym);benzo[1,2-c,3,4-c']bis[1,2,5]oxadiazole 1(or 3),6-dioxide;

Chemical Property of benzo(1,2-c:3,4-c')bis(1,2,5)oxadiazole-1,6-dioxide

Chemical Property:

• Vapor Pressure: 2.17E-18mmHg at 25°C
• Boiling Point: 424.2°Cat760mmHg
• Flash Point: 210.4°C
• PSA: 102.98000
• Density: 2.36g/cm³
• LogP: 0.82600

Purity/Quality:

FUROXANOBENZOFUROXAN 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzo(1,2-c:3,4-c')bis(1,2,5)oxadiazole-1,6-dioxide

There total 6 articles about benzo(1,2-c:3,4-c')bis(1,2,5)oxadiazole-1,6-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-chloro-2,4-dinitrochlorobenzene (10199-85-6) → benzo[1,2-c;3,4-c']bis[1,2,5]oxadiazole 1,6-dioxide (5714-12-5)

Guidance literature:

With sodium azide; N-ethyl-N-methylpyrrolidinium tetrafluoroborate; tetrabutylammomium bromide; In water; at 55 ℃; for 1h;

DOI:10.1016/j.mencom.2012.03.015

Reference yield:

4-Nitro-5-chlorobenzofuroxane (18378-14-8) → benzo[1,2-c;3,4-c']bis[1,2,5]oxadiazole 1,6-dioxide (5714-12-5)

Guidance literature:

With sodium azide; In methanol;

DOI:10.1021/jm00248a013

Reference yield:

5-azido-4-nitro-benzo[1,2,5]oxadiazole 1-oxide → benzo[1,2-c;3,4-c']bis[1,2,5]oxadiazole 1,6-dioxide (5714-12-5)

Guidance literature:

In acetic acid;

DOI:10.1021/jm00308a027

upstream raw materials:

4-Nitro-5-chlorobenzofuroxane

5-chloro-4-nitrobenzofuroxan

1-chloro-2,4-dinitrochlorobenzene