Technology Process of 1-NITROFLUORENE
There total 10 articles about 1-NITROFLUORENE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: 2.) 2 M aq. Na2CO3 / 1.) Pd(PPh3)4 / 1.) EtOH, DME, 10 min, 2.) reflux, 20 h
2: 94 percent / NBS / benzoyl peroxide / CCl4 / 36 h / Heating
3: KOAc / 4 h / Heating
4: 1 N aq. NaOH / ethanol; tetrahydrofuran / 12 h / Ambient temperature
5: 86 percent / polyphosphoric acid / 26 h / Heating
With
sodium hydroxide; N-Bromosuccinimide; PPA; potassium acetate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0); dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; ethanol;
DOI:10.1055/s-1989-27189
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / NBS / benzoyl peroxide / CCl4 / 36 h / Heating
2: KOAc / 4 h / Heating
3: 1 N aq. NaOH / ethanol; tetrahydrofuran / 12 h / Ambient temperature
4: 86 percent / polyphosphoric acid / 26 h / Heating
With
sodium hydroxide; N-Bromosuccinimide; PPA; potassium acetate;
dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; ethanol;
DOI:10.1055/s-1989-27189
