5-Cyclotetradecen-1-ol, (Z)-

Base Information

• Chemical Name: 5-Cyclotetradecen-1-ol, (Z)-
• CAS No.: 114157-34-5
• Molecular Formula: C14H26O
• Molecular Weight: 210.36

Synonyms:

Chemical Property of 5-Cyclotetradecen-1-ol, (Z)-

Chemical Property:

Purity/Quality:

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Technology Process of 5-Cyclotetradecen-1-ol, (Z)-

There total 1 articles about 5-Cyclotetradecen-1-ol, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-bromoheptanal (54005-84-4) → (Z)-Cyclotetradec-5-enol (114157-34-5)

Guidance literature:

Multi-step reaction with 7 steps

1: 71 percent / tetrahydrofuran / 0.03 h / 0 °C

2: PCC, celite / CH₂Cl₂ / 3 h / Ambient temperature

3: tetrahydrofuran / 0.5 h / -78 °C

4: Jones reagent / acetone / 0.08 h

5: sodium iodide / butan-2-one / 3 h / Heating

6: 75 percent / tributyltin hydride, AIBN / benzene / 3 h / Heating

7: 91 percent / NaBH₄

With sodium tetrahydroborate; jones reagent; 2,2'-azobis(isobutyronitrile); Celite; tri-n-butyl-tin hydride; pyridinium chlorochromate; sodium iodide; In tetrahydrofuran; dichloromethane; acetone; butanone; benzene;

DOI:10.1021/ja00219a034

Reference yield:

(Z)-Cyclotetradec-5-enol (114157-34-5) → cis-cyclotetradecene (2484-64-2,6568-33-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / 2-chloro-3-ethylbenzoxazolium tetrafluoroborate, tetraethylammonium bromide / -78 °C

2: tributyltin hydride / benzene / 80 °C

With 3-ethyl-2-chlorobenzoxazolium tetrafluoroborate; tetraethylammonium bromide; tri-n-butyl-tin hydride; In benzene;

DOI:10.1021/ja00219a034

upstream raw materials:

7-bromoheptanal

Downstream raw materials:

cis-cyclotetradecene

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