13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene

Base Information

Chemical Name:13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene
CAS No.:73650-69-8
Molecular Formula:C₁₂H₁₂S₂
Molecular Weight:220.359
Hs Code.:
DSSTox Substance ID:DTXSID70223865
Nikkaji Number:J682.462E
Wikidata:Q83102361

Synonyms:73650-69-8;13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene;13,14-Dithiatricyclo[8.2.1.14,7]tetradeca-4,6,10,12-tetraene;[2.2](2,5)thiophenophane;DTXSID70223865;7075-88-9;13,14-Dithiatricyclo[8.2.1.14,7]- tetradeca-4,6,10,12-tetraene

Suppliers and Price of 13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene

Chemical Property:

Vapor Pressure:0.000331mmHg at 25°C
Boiling Point:329.9°C at 760 mmHg
Flash Point:113.6°C
PSA：56.48000
Density:1.22g/cm³
LogP:3.69340
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:220.03804273
Heavy Atom Count:14
Complexity:163

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC=C(S2)CCC3=CC=C1S3

Technology Process of 13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene

There total 5 articles about 13,14-Dithiatricyclo(8.2.1.14,7)tetradeca-4,6,10,12-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.3%

: 66806-34-6
2,5-dimethylene-2,5-dihydrothiophene

: 7075-88-9,73650-69-8
[2.2]thiophenophane

: 65038-09-7
19,20,21-trithiatetracyclo[14.2.1.1^3.6.1^9,12]heneicosa-4,6,10,12,16,18-hexaene

Guidance literature:: In carbon disulfide; chloroform-d1; Ambient temperature;
DOI:10.1021/jo961528i

Reference yield: 17.0%

: 76233-25-5
<5-<(trimethylsilyl)methyl>thenyl>trimethylammonium iodide

: 7075-88-9,73650-69-8
[2.2]thiophenophane

: 65038-09-7
19,20,21-trithiatetracyclo[14.2.1.1^3.6.1^9,12]heneicosa-4,6,10,12,16,18-hexaene

Guidance literature:: With cesium fluoride; In acetonitrile; Heating;
DOI:10.1021/jo00318a047

Reference yield:

: 13314-90-4
2,5-dimethylene-2,5-dihydro-furan

: 5088-46-0,73650-68-7
[2.2](2.5)furanocyclophane

: 25201-17-6
13-oxa-14-thiatricyclo[8.2.1.1^3,6]tetradeca-4,6,10,12-tetraene

: 7075-88-9,73650-69-8
[2.2]thiophenophane

: 19-oxa-20,21-dithiatetracyclo[14.2.1.1^3.6.1^9,12]heneicosa-4,6,10,12,16,18-hexaene

Guidance literature:: With 2,5-dimethylene-2,5-dihydrothiophene; Yield given. Further byproducts given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo961528i