cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol

Base Information

Chemical Name:cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol
CAS No.:66934-76-7
Molecular Formula:C₁₁H₁₂O
Molecular Weight:160.216
Hs Code.:
DSSTox Substance ID:DTXSID70985613
Nikkaji Number:J1.959.565J
Wikidata:Q76154904

Synonyms:BRN 2047571;cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol;66934-76-7;3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol, 1,2,3,7b-tetrahydro-, cis-;DTXSID70985613;LS-57748;1,2,3,7b-Tetrahydro-3aH-cyclopenta[3,4]cyclobuta[1,2]benzen-3a-ol

Suppliers and Price of cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol

Chemical Property:

Vapor Pressure:0.000757mmHg at 25°C
Boiling Point:294°Cat760mmHg
Flash Point:105.7°C
Density:1.263g/cm³
XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:160.088815002
Heavy Atom Count:12
Complexity:201

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2C3=CC=CC=C3C2(C1)O
Isomeric SMILES:C1C[C@@H]2C3=CC=CC=C3[C@@]2(C1)O

Technology Process of cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol

There total 3 articles about cis-1,2,3,7b-Tetrahydro-3aH-cyclopenta(3,4)cyclobuta(1,2)benzen-3a-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 120-92-3
cyclopentanone

: 1198-34-1
2-Phenylcyclopentanone

: 66934-76-7
1,2,3,7b-tetrahydro-3aH-cyclopenta[3,4]cyclobuta[1,2]benzen-3a-ol

Guidance literature:: cyclopentanone; With tetramethylpiperidine; tert.-butyl lithium; In tetrahydrofuran; hexane; at -40 ℃;

halobenzene; In tetrahydrofuran; hexane; at -40 ℃; for 5h;
DOI:10.1139/v03-099

Reference yield: 34.0%

: 108-86-1,52753-63-6
bromobenzene

: 120-92-3
cyclopentanone

: 66934-76-7
1,2,3,7b-tetrahydro-3aH-cyclopenta[3,4]cyclobuta[1,2]benzen-3a-ol

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 5h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.9b03652