Pyridinium, 1-methyl-4-(phenylacetyl)-, bromide

Base Information

Chemical Name:Pyridinium, 1-methyl-4-(phenylacetyl)-, bromide
CAS No.:114443-53-7
Molecular Formula:C14H14NO.Br
Molecular Weight:292.175
Hs Code.:

Synonyms:

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Chemical Property of Pyridinium, 1-methyl-4-(phenylacetyl)-, bromide

Chemical Property:

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Technology Process of Pyridinium, 1-methyl-4-(phenylacetyl)-, bromide

There total 9 articles about Pyridinium, 1-methyl-4-(phenylacetyl)-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2459-09-8
4-pyridinecarboxylic acid, methyl ester

: 114443-53-7
1-Methyl-4-phenylacetyl-pyridinium; bromide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium ethoxide / ethanol / 2 h / Heating

2: hydrobromic acid / propan-2-ol; diethyl ether / 12 h / Heating

3: aqueous sodium bicarbonate

4: acetone / 24 h / Ambient temperature

With hydrogen bromide; sodium ethanolate; sodium hydrogencarbonate; In diethyl ether; ethanol; isopropyl alcohol; acetone;
DOI:10.1021/ja00220a046

Reference yield:

: 27768-46-3
N-(pyridin-4-ylmethylene)aniline

: 114443-53-7
1-Methyl-4-phenylacetyl-pyridinium; bromide

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol; diethyl ether

2: 50 percent / 10percent methanolic potassium hydroxide / tetrahydrofuran; diethyl ether; acetone / -40 °C

3: conc. hydrochloric acid / ethanol

4: aqueous sodium bicaebonate

5: acetone / 24 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; ethanol; acetone;
DOI:10.1021/ja00220a046

Reference yield:

: 140-29-4
phenylacetonitrile

: 114443-53-7
1-Methyl-4-phenylacetyl-pyridinium; bromide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium ethoxide / ethanol / 2 h / Heating

2: hydrobromic acid / propan-2-ol; diethyl ether / 12 h / Heating

3: aqueous sodium bicarbonate

4: acetone / 24 h / Ambient temperature

With hydrogen bromide; sodium ethanolate; sodium hydrogencarbonate; In diethyl ether; ethanol; isopropyl alcohol; acetone;
DOI:10.1021/ja00220a046