L-Leucinamide, N-[(1,1-dimethylethoxy)carbonyl]glycyl-L-phenylalanyl-N-[1-(hydroxymeth yl)-4-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]-, (S)-

Base Information

Chemical Name:L-Leucinamide, N-[(1,1-dimethylethoxy)carbonyl]glycyl-L-phenylalanyl-N-[1-(hydroxymeth yl)-4-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]-, (S)-
CAS No.:114475-79-5
Molecular Formula:C₃₇H₅₇N₇O₈S
Molecular Weight:759.968
Hs Code.:
Mol file:114475-79-5.mol

L-Leucinamide,
N-[(1,1-dimethylethoxy)carbonyl]glycyl-L-phenylalanyl-N-[1-(hydroxymeth
yl)-4-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]-,
(S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Leucinamide, N-[(1,1-dimethylethoxy)carbonyl]glycyl-L-phenylalanyl-N-[1-(hydroxymeth yl)-4-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]-, (S)-

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Technology Process of L-Leucinamide, N-[(1,1-dimethylethoxy)carbonyl]glycyl-L-phenylalanyl-N-[1-(hydroxymeth yl)-4-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]-, (S)-

There total 1 articles about L-Leucinamide, N-[(1,1-dimethylethoxy)carbonyl]glycyl-L-phenylalanyl-N-[1-(hydroxymeth yl)-4-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 114475-78-4
Boc-Gly-Phe-Leu-Arg(Mts)-OMe

: 114475-79-5
Boc-Gly-Phe-Leu-Arg(Mts)-ol

Guidance literature:: With sodium tetrahydroborate;
DOI:10.1248/cpb.35.2561

Reference yield:

: 114475-79-5
Boc-Gly-Phe-Leu-Arg(Mts)-ol

: 114475-59-1
H-Tyr-D-Arg-Gly-Phe-Leu-Arg-ol

Guidance literature:: Multi-step reaction with 2 steps

2: 33 percent / TFMSA

With trifluorormethanesulfonic acid;
DOI:10.1248/cpb.35.2561