4-Oxazolecarboxamide, N-[4-[[2,3-bis(phenylmethoxy)benzoyl]amino]butyl]-N-[3-[[2,3-bis(phenyl methoxy)benzoyl]amino]propyl]-2-methyl-

Base Information

Chemical Name:4-Oxazolecarboxamide, N-[4-[[2,3-bis(phenylmethoxy)benzoyl]amino]butyl]-N-[3-[[2,3-bis(phenyl methoxy)benzoyl]amino]propyl]-2-methyl-
CAS No.:114482-47-2
Molecular Formula:C54H54N4O8
Molecular Weight:887.045
Hs Code.:
Mol file:114482-47-2.mol

Synonyms:

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Chemical Property of 4-Oxazolecarboxamide, N-[4-[[2,3-bis(phenylmethoxy)benzoyl]amino]butyl]-N-[3-[[2,3-bis(phenyl methoxy)benzoyl]amino]propyl]-2-methyl-

Chemical Property:

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Technology Process of 4-Oxazolecarboxamide, N-[4-[[2,3-bis(phenylmethoxy)benzoyl]amino]butyl]-N-[3-[[2,3-bis(phenyl methoxy)benzoyl]amino]propyl]-2-methyl-

There total 6 articles about 4-Oxazolecarboxamide, N-[4-[[2,3-bis(phenylmethoxy)benzoyl]amino]butyl]-N-[3-[[2,3-bis(phenyl methoxy)benzoyl]amino]propyl]-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 23012-17-1
2-methyl-1,3-oxazol-4-carboxylic acid

: 74272-81-4
2,3-bis(benzyloxy)-N-(3-(4-(2,3-bis(benzyloxy)benzamido)butylamino)propyl)benzamide

: 114482-47-2
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-methyloxazole-4-carboxamide

Guidance literature:: With dmap; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; for 72h; Ambient temperature;

Reference yield:

: 2411-83-8
methyl-2,3-dihydroxybenzoate

: 114482-47-2
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-methyloxazole-4-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / K₂CO₃ / dimethylformamide / Ambient temperature

2: 83 percent / 40percent KOH / H₂O; tetrahydrofuran

3: dicyclohexylcarbodi-imide/DMAP / CHCl₃ / Ambient temperature

4: 79 percent / CH₂Cl₂ / 3 h / Ambient temperature

5: 74 percent / diphenylphosphoryl azide/Et₃N,DMAP / dimethylformamide / 72 h / Ambient temperature

With dmap; potassium hydroxide; diphenylphosphoranyl azide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 303-38-8
2,3-Dihydroxybenzoic acid

: 114482-47-2
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-2-methyloxazole-4-carboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / H₂SO₄ / 20 h / Heating

2: 98 percent / K₂CO₃ / dimethylformamide / Ambient temperature

3: 83 percent / 40percent KOH / H₂O; tetrahydrofuran

4: dicyclohexylcarbodi-imide/DMAP / CHCl₃ / Ambient temperature

5: 79 percent / CH₂Cl₂ / 3 h / Ambient temperature

6: 74 percent / diphenylphosphoryl azide/Et₃N,DMAP / dimethylformamide / 72 h / Ambient temperature

With dmap; potassium hydroxide; sulfuric acid; diphenylphosphoranyl azide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; chloroform; water; N,N-dimethyl-formamide;