Technology Process of Oxiranebutanoic acid, 3-(hydroxymethyl)-, methyl ester, cis-
There total 15 articles about Oxiranebutanoic acid, 3-(hydroxymethyl)-, methyl ester, cis- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 23 ℃;
for 2h;
DOI:10.1021/ja00524a045
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 96 percent / benzoic acid / 1,2-dimethoxy-ethane / 4 h / Heating
2: 100 percent / H2SO4 / 3 h / 23 °C
3: 93 percent / 95percent zinc amalgam, dry hydrogen chloride / diethyl ether / 6 h / 15 °C
4: 100 percent / H2 / 10percent Pd/C / methanol / 23 °C
5: 99 percent / dry hydroden chloride / 72 h / 23 °C
6: 98 percent / pyridine / 1.) 23 deg C, 6 h, 2.) 50 deg C, 3h
7: 98 percent / K2CO3 / methanol / 2 h / 23 °C
With
pyridine; hydrogenchloride; amalgamated zinc; sulfuric acid; hydrogen; potassium carbonate; benzoic acid;
palladium on activated charcoal;
In
methanol; 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/ja00524a045
