DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, phenylmethyl ester, mono(4-methylbenzenesulfonate)

Base Information

Chemical Name:DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, phenylmethyl ester, mono(4-methylbenzenesulfonate)
CAS No.:114531-70-3
Molecular Formula:C₇H₈O₃S*C₂₉H₂₈N₄O₅S
Molecular Weight:716.836
Hs Code.:
Mol file:114531-70-3.mol

DL-Phenylalanine,
3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-,
phenylmethyl ester, mono(4-methylbenzenesulfonate)

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Chemical Property of DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, phenylmethyl ester, mono(4-methylbenzenesulfonate)

Chemical Property:

Purity/Quality:

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Technology Process of DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, phenylmethyl ester, mono(4-methylbenzenesulfonate)

There total 6 articles about DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, phenylmethyl ester, mono(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 104-15-4
toluene-4-sulfonic acid

: 114531-56-5
Nα-(2-Naphthylsulfonylglycyl)-3-amidinophenylalanin

: 100-51-6,185532-71-2
benzyl alcohol

: 114531-70-3
3-(3-Carbamimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionic acid benzyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: for 5h; Heating;

Reference yield:

: 63999-80-4
(+/-)-3-cyanophenylalanine

: 114531-70-3
3-(3-Carbamimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionic acid benzyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / 1M NaOH / ethyl acetate / 4 h / Ambient temperature

2: 95 percent / H₂S / pyridine; triethylamine / 48 h / Ambient temperature

3: 87 percent / acetone / 0.25 h / Heating

4: 77 percent / CH₃COONH₄ / methanol / 2.5 h / 60 °C

5: 74 percent / 5 h / Heating

With sodium hydroxide; hydrogen sulfide; ammonium acetate; In pyridine; methanol; ethyl acetate; triethylamine; acetone;

Reference yield:

: 92740-50-6
2-Naphthylsulfonylglycylchlorid

: 114531-70-3
3-(3-Carbamimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionic acid benzyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / 1M NaOH / ethyl acetate / 4 h / Ambient temperature

2: 95 percent / H₂S / pyridine; triethylamine / 48 h / Ambient temperature

3: 87 percent / acetone / 0.25 h / Heating

4: 77 percent / CH₃COONH₄ / methanol / 2.5 h / 60 °C

5: 74 percent / 5 h / Heating

With sodium hydroxide; hydrogen sulfide; ammonium acetate; In pyridine; methanol; ethyl acetate; triethylamine; acetone;