see 1,14-Dioxacyclohexacosane-2,15-dione

Base Information

• Chemical Name: see 1,14-Dioxacyclohexacosane-2,15-dione
• CAS No.: 807-04-5
• Molecular Formula: C₂₄H₄₄O₄
• Molecular Weight: 396.611
• Mol file: 807-04-5.mol

Synonyms:

Chemical Property of see 1,14-Dioxacyclohexacosane-2,15-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of see 1,14-Dioxacyclohexacosane-2,15-dione

There total 2 articles about see 1,14-Dioxacyclohexacosane-2,15-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

Acrylic acid 9-iodo-nonyl ester (133123-00-9) → oxacyclotridecan-2-one (947-05-7) + n-nonyl acrylate (2664-55-3) + 1,14-dioxacyclohexacosane-2,15-dione (807-04-5)

Guidance literature:

With sodium cyanoborohydride; In methanol; for 3h; Ambient temperature; Irradiation;

DOI:10.1246/cl.1994.1789

Reference yield:

9-bromononan-1-ol (55362-80-6) → 1,14-dioxacyclohexacosane-2,15-dione (807-04-5)

Guidance literature:

Multi-step reaction with 3 steps

1: NaI / acetone / Ambient temperature

2: p-TolSO₃H / benzene / Heating

3: 11 percent Chromat_. / NaBH₃CN / methanol / 3 h / Ambient temperature; Irradiation

With sodium cyanoborohydride; toluene-4-sulfonic acid; sodium iodide; In methanol; acetone; benzene;

DOI:10.1246/cl.1994.1789

upstream raw materials:

Acrylic acid 9-iodo-nonyl ester

9-bromononan-1-ol