2,2'-((4-Amino-3-nitrophenyl)imino)bisethanol

Base Information

• Chemical Name: 2,2'-((4-Amino-3-nitrophenyl)imino)bisethanol
• CAS No.: 29705-39-3
• Molecular Formula: C10H15 N3 O4
• Molecular Weight: 241.247
• Hs Code.: 2922199090
• DSSTox Substance ID: DTXSID10183853
• Nikkaji Number: J365.413C
• Wikidata: Q81985496
• Mol file: 29705-39-3.mol

Synonyms:29705-39-3;2,2'-((4-Amino-3-nitrophenyl)imino)bisethanol;2,2'-[(4-Amino-3-nitrophenyl)imino]bisethanol;2,2'-[(4-Amino-3-nitrophenyl)imino]diethanol;Ethanol, 2,2'-((4-amino-3-nitrophenyl)imino)bis-;Ethanol, 2,2'-[(4-amino-3-nitrophenyl)imino]bis-;SCHEMBL127252;DTXSID10183853;FT-0713817;2,2'-[(4-AMINO-3-NITROPHENYL)IMINO]BIS-ETHANOL

Chemical Property of 2,2'-((4-Amino-3-nitrophenyl)imino)bisethanol

Chemical Property:

• Boiling Point: 499°Cat760mmHg
• Flash Point: 255.6°C
• PSA: 115.54000
• Density: 1.422g/cm³
• LogP: 1.07240
• XLogP3: 0
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 241.10625597
• Heavy Atom Count: 17
• Complexity: 240

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1N(CCO)CCO)[N+](=O)[O-])N

Technology Process of 2,2'-((4-Amino-3-nitrophenyl)imino)bisethanol

There total 3 articles about 2,2'-((4-Amino-3-nitrophenyl)imino)bisethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2’-[4-(2-hydroxyethylamino)-3-nitrophenylimino]diethanol (33229-34-4) → 2-nitro-1-amino-4-[bis-(2-hydroxyethyl)-amino]-benzene (29705-39-3)

Guidance literature:

With ammonium hydroxide; sodium sulfite; In methanol; at 70 ℃; for 144h;

DOI:10.1016/S0040-4020(98)00181-1

Reference yield: 10.0%

2,5-bis(2-hydroxyethyl)-amino-nitrobenzene (84041-77-0) → 2-nitro-1-amino-4-[bis-(2-hydroxyethyl)-amino]-benzene (29705-39-3) + 2-hydroxy-5-N-(2'-hydroxyethyl)amino-1-nitrobenzene (165672-32-2)

Guidance literature:

With ammonium hydroxide; sodium sulfite; In methanol; at 70 ℃; for 24h;

DOI:10.1016/S0040-4020(98)00181-1

Reference yield:

→ 2-nitro-1-amino-4-[bis-(2-hydroxyethyl)-amino]-benzene (29705-39-3)

Guidance literature:

upstream raw materials:

2,2’-[4-(2-hydroxyethylamino)-3-nitrophenylimino]diethanol

2,5-bis(2-hydroxyethyl)-amino-nitrobenzene

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