2,5-Piperazinedione, 3-[[2-(1,1-dimethyl-2-propenyl)-1H-indol-3-yl]methyl]-6-methylene-4-[[(4- methylphenyl)sulfonyl]oxy]-1-(2-propenyl)-

Base Information

Chemical Name:2,5-Piperazinedione, 3-[[2-(1,1-dimethyl-2-propenyl)-1H-indol-3-yl]methyl]-6-methylene-4-[[(4- methylphenyl)sulfonyl]oxy]-1-(2-propenyl)-
CAS No.:114705-67-8
Molecular Formula:C29H31N3O5S
Molecular Weight:533.648
Hs Code.:
Mol file:114705-67-8.mol

Synonyms:

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Chemical Property of 2,5-Piperazinedione, 3-[[2-(1,1-dimethyl-2-propenyl)-1H-indol-3-yl]methyl]-6-methylene-4-[[(4- methylphenyl)sulfonyl]oxy]-1-(2-propenyl)-

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Technology Process of 2,5-Piperazinedione, 3-[[2-(1,1-dimethyl-2-propenyl)-1H-indol-3-yl]methyl]-6-methylene-4-[[(4- methylphenyl)sulfonyl]oxy]-1-(2-propenyl)-

There total 5 articles about 2,5-Piperazinedione, 3-[[2-(1,1-dimethyl-2-propenyl)-1H-indol-3-yl]methyl]-6-methylene-4-[[(4- methylphenyl)sulfonyl]oxy]-1-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 114519-52-7
2-allyl-2'-(α,α-dimethylallyl)-5-hydroxy-1-methylspiro<2,5-diazabicyclo-<2.2.2>octane-7,3'-<3'H>indole>-3,6-dione

: 98-59-9
p-toluenesulfonyl chloride

: 114705-67-8
1-allyl-3-<2-(α,α-dimethylallyl)indol-3-ylmethyl>-6-methylene-4-tosyloxypiperazine-2,5-dione

Guidance literature:: With triethylamine; In dichloromethane; for 2h;

Reference yield:

: 114519-39-0
(E)-N-allyl-β-<2-(α,α-dimethylallyl)indol-3-yl>-α-(hydroxyimino)propanamide

: 114705-67-8
1-allyl-3-<2-(α,α-dimethylallyl)indol-3-ylmethyl>-6-methylene-4-tosyloxypiperazine-2,5-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / 7 M HCl, TMA*BH₃ / ethanol / 18 h / Ambient temperature

2: CH₂Cl₂ / 0.25 h

3: CF₃CO₂H / CH₂Cl₂ / 72 h / Ambient temperature

4: 90 percent / triethylamine / CH₂Cl₂ / 2 h

With hydrogenchloride; tetramethylammonium; borane; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane;

Reference yield:

: 108782-34-9
ethyl (E)-β-<2-(α,α-dimethylallyl)indol-3-yl-α-(hydroxyimino)>propanoate

: 114705-67-8
1-allyl-3-<2-(α,α-dimethylallyl)indol-3-ylmethyl>-6-methylene-4-tosyloxypiperazine-2,5-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / 2.0 M trimethylaluminium / hexane; CH₂Cl₂ / 3 h / 35 °C

2: 84 percent / 7 M HCl, TMA*BH₃ / ethanol / 18 h / Ambient temperature

3: CH₂Cl₂ / 0.25 h

4: CF₃CO₂H / CH₂Cl₂ / 72 h / Ambient temperature

5: 90 percent / triethylamine / CH₂Cl₂ / 2 h

With hydrogenchloride; tetramethylammonium; borane; trimethylaluminum; triethylamine; trifluoroacetic acid; In ethanol; hexane; dichloromethane;