Benzenethiol, 4-(decyloxy)-

Base Information

• Chemical Name: Benzenethiol, 4-(decyloxy)-
• CAS No.: 114833-57-7
• Molecular Formula: C₁₆H₂₆OS
• Molecular Weight: 266.448
• Mol file: 114833-57-7.mol

Synonyms:

Chemical Property of Benzenethiol, 4-(decyloxy)-

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenethiol, 4-(decyloxy)-

There total 5 articles about Benzenethiol, 4-(decyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.4%

S-(4-decyloxyphenyl)-N,N-dimethylthiocarbamate (114833-56-6) → 4-n-decyloxythiophenol (114833-57-7)

Guidance literature:

With sodium hydroxide; In methanol; water; for 8h; Heating;

Reference yield:

4-decyloxyphenol (35108-00-0) → 4-n-decyloxythiophenol (114833-57-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 84.3 percent / 80 percent NaH in oil / dimethylformamide / 1.) room temperature, 1 h; 2.) heating, 1 h, 70 deg C

2: 0.5 h / 315 °C

3: 51.4 percent / NaOH / H₂O; methanol / 8 h / Heating

With sodium hydroxide; sodium hydride; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

O-(4-decyloxyphenyl)-N,N-dimethylthiocarbamate (114833-34-0) → 4-n-decyloxythiophenol (114833-57-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.5 h / 315 °C

2: 51.4 percent / NaOH / H₂O; methanol / 8 h / Heating

With sodium hydroxide; In methanol; water;

upstream raw materials:

S-(4-decyloxyphenyl)-N,N-dimethylthiocarbamate

4-decyloxyphenol

O-(4-decyloxyphenyl)-N,N-dimethylthiocarbamate

Refernces

• 1、 Neubert, Mary E.,Ziemnicka-Merchant, Barbara,Jirousek, Michael R.,Laskos, Stanley J.,Leonhardt, Darrin,Sharma, Ram B.. "The Effect of Two Terminal Alkoxy Groups on the Mesomorphic Properties of 4,4'-Disubstituted Phenylthiobenzoates". . p. 209 - 240. Retrieved 2007/10/02.