3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]-

Base Information

Chemical Name:3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]-
CAS No.:114856-95-0
Molecular Formula:C15H20N4O3
Molecular Weight:304.349
Hs Code.:

Synonyms:3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]-

Suppliers and Price of 3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]-

There total 6 articles about 3(2H)-Pyridazinone,4,5-dihydro-5-methyl-6-[4-[(2-methyl-2-nitropropyl)amino]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.2%

: 184766-13-0
3-[4-(2-methyl-2-nitropropylamino)benzoyl]butyric acid

: 114856-95-0
6-[4-(2-methyl-2-nitropropylamino)phenyl]-5-methyl-4,5-dihydro-3(2H)-pyridazinone

Guidance literature:: With hydrazine hydrate; at 100 ℃; for 3h;
DOI:10.1248/cpb.44.2061

Reference yield:

: 114856-94-9
γ-[4-(2-methyl-2-nitropropylamino)benzoyl]butyric acid

: 114856-95-0
6-[4-(2-methyl-2-nitropropylamino)phenyl]-5-methyl-4,5-dihydro-3(2H)-pyridazinone

Guidance literature:: With hydrazine hydrate; In water;

Reference yield:

: 122-85-0
para-acetamidobenzaldehyde

: 114856-95-0
6-[4-(2-methyl-2-nitropropylamino)phenyl]-5-methyl-4,5-dihydro-3(2H)-pyridazinone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) p-TsOH*H₂O / 1.) THF, reflux, 1 h, 2.) THF, H₂O, reflux, 3 h

2: benzyltriethylammonium chloride, KOH / dimethylformamide / 6 h / Ambient temperature

3: 89.9 percent / aq. AcOH / 2 h / 100 °C

4: 68.8 percent / 2N aq. HCl / 2 h / Heating

5: 82.8 percent / benzyltriethylammonium chloride, aq. NaOH / 8 h / Heating

6: 88.2 percent / aq. hydrazine hydrate / 3 h / 100 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.44.2061