1-[1-(Chloromethyl)cyclohexyl]ethan-1-one

Base Information

Chemical Name:1-[1-(Chloromethyl)cyclohexyl]ethan-1-one
CAS No.:115437-03-1
Molecular Formula:C9H15ClO
Molecular Weight:174.671
Hs Code.:
DSSTox Substance ID:DTXSID90560901
Wikidata:Q82444538

Synonyms:115437-03-1;1-[1-(Chloromethyl)cyclohexyl]ethan-1-one;DTXSID90560901

Suppliers and Price of 1-[1-(Chloromethyl)cyclohexyl]ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[1-(Chloromethyl)cyclohexyl]ethan-1-one

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:174.0811428
Heavy Atom Count:11
Complexity:148

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1(CCCCC1)CCl

Technology Process of 1-[1-(Chloromethyl)cyclohexyl]ethan-1-one

There total 3 articles about 1-[1-(Chloromethyl)cyclohexyl]ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160193-87-3
1-Acetyl-1-((mesyloxy)methyl)cyclohexane

: 115437-03-1
1-(1-Chloromethyl-cyclohexyl)-ethanone

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; for 15h; Yield given; Heating;
DOI:10.1021/jo00102a022

Reference yield:

: 823-76-7
Cyclohexyl methyl ketone

: 115437-03-1
1-(1-Chloromethyl-cyclohexyl)-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 7 h / Heating

2: 15percent aq. Na₂CO₃ / 96 h / Ambient temperature

3: pyridine / CH₂Cl₂ / 24 h / Ambient temperature

4: LiCl / dimethylformamide / 15 h / Heating

With pyridine; sodium carbonate; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00102a022

Reference yield:

: 215876-63-4
Trifluoro-acetic acid 1-acetyl-cyclohexylmethyl ester

: 115437-03-1
1-(1-Chloromethyl-cyclohexyl)-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 15percent aq. Na₂CO₃ / 96 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 24 h / Ambient temperature

3: LiCl / dimethylformamide / 15 h / Heating

With pyridine; sodium carbonate; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00102a022