2H-1,5-Benzodioxepin-6-amine, 3,4-dihydro-, hydrochloride

Base Information

Chemical Name:2H-1,5-Benzodioxepin-6-amine, 3,4-dihydro-, hydrochloride
CAS No.:115464-85-2
Molecular Formula:C9H11NO2.ClH
Molecular Weight:201.653
Hs Code.:
Mol file:115464-85-2.mol

Synonyms:

Suppliers and Price of 2H-1,5-Benzodioxepin-6-amine, 3,4-dihydro-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 2H-1,5-Benzodioxepin-6-amine, 3,4-dihydro-, hydrochloride

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2H-1,5-Benzodioxepin-6-amine, 3,4-dihydro-, hydrochloride

There total 1 articles about 2H-1,5-Benzodioxepin-6-amine, 3,4-dihydro-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6665-98-1
3-nitrobenzene-1,2-diol

: 115464-85-2
6-amino-3,4-dihydro-2H-1,5-benzodioxepine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, Bu₄NBr / toluene / 24 h / 80 °C

2: 89 percent / H₂, 12 N HCl / 10percent Pd/C / ethanol / 1.5 h / 20 °C / 760 Torr

With hydrogenchloride; tetrabutylammomium bromide; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; toluene;
DOI:10.1021/jm00118a011

Reference yield: 51.0%

: 821-48-7
bis-(2-chloroethyl)amine hydrochloride

: 115464-85-2
6-amino-3,4-dihydro-2H-1,5-benzodioxepine hydrochloride

: 115464-82-9
1-(3,4-dihydro-2H-1,5-benzodioxepin-6-yl)piperazine dihydrochloride

Guidance literature:: With hydrogenchloride; In chlorobenzene; for 60h; Heating;
DOI:10.1021/jm00118a011

Reference yield:

: 115464-85-2
6-amino-3,4-dihydro-2H-1,5-benzodioxepine hydrochloride

: 114518-11-5
1-(5-phenylpyrrol-2-yl)methyl-4-(2H-3,4-dihydrobenzo-1,5-dioxepin-6-yl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / 2.) HCl / chlorobenzene / 60 h / Heating

2: 55 percent / ethanol; H₂O / 4 h / Heating

With hydrogenchloride; In ethanol; water; chlorobenzene;
DOI:10.1021/jm00118a011