{[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane)

Base Information

Chemical Name:{[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane)
CAS No.:115820-49-0
Molecular Formula:C₁₇H₃₅IOSi₄
Molecular Weight:494.711
Hs Code.:
DSSTox Substance ID:DTXSID30766268

Synonyms:115820-49-0;DTXSID30766268;{[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane)

Suppliers and Price of {[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane)

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:493.07314
Heavy Atom Count:23
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)[Si](C([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)I

Technology Process of {[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane)

There total 4 articles about {[Iodo(4-methoxyphenyl)silyl]methanetriyl}tris(trimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 115820-45-6
1-Methoxy-4-[(tris-trimethylsilanyl-methyl)-silanyl]-benzene

: 115820-49-0
1-[Iodo-(tris-trimethylsilanyl-methyl)-silanyl]-4-methoxy-benzene

Guidance literature:: With Iodine monochloride; In tetrachloromethane; for 0.0833333h; Ambient temperature;
DOI:10.1016/0022-328X(87)80272-3

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 115820-49-0
1-[Iodo-(tris-trimethylsilanyl-methyl)-silanyl]-4-methoxy-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / diethyl ether; hexane / 2 h / Ambient temperature

2: 60 percent / ICl / CCl₄ / 0.08 h / Ambient temperature

With Iodine monochloride; In tetrachloromethane; diethyl ether; hexane;
DOI:10.1016/0022-328X(87)80272-3

Reference yield:

: 72190-68-2
(Me₃Si)3CSiH₂I

: 115820-49-0
1-[Iodo-(tris-trimethylsilanyl-methyl)-silanyl]-4-methoxy-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / silver tetrafluoroborate / diethyl ether / 0.17 h / Ambient temperature

2: 90 percent / diethyl ether; hexane / 2 h / Ambient temperature

3: 60 percent / ICl / CCl₄ / 0.08 h / Ambient temperature

With silver tetrafluoroborate; Iodine monochloride; In tetrachloromethane; diethyl ether; hexane;
DOI:10.1016/0022-328X(87)80272-3