Bis[1-(3-nitrophenyl)ethylidene]hydrazine

Base Information

Chemical Name:Bis[1-(3-nitrophenyl)ethylidene]hydrazine
CAS No.:5340-12-5
Molecular Formula:C16H14N4O4
Molecular Weight:326.312
Hs Code.:
NSC Number:866

Synonyms:bis[1-(3-nitrophenyl)ethylidene]hydrazine;5340-12-5;(E)-1-(3-nitrophenyl)-N-[(E)-1-(3-nitrophenyl)ethylideneamino]ethanimine;NSC866;NSC-866;3'-NITROACETOPHENONE, AZINE;CCG-52605;SR-01000641828-1;(1E,2E)-1,2-Bis[1-(3-nitrophenyl)ethylidene]hydrazine

Suppliers and Price of Bis[1-(3-nitrophenyl)ethylidene]hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Bis[1-(3-nitrophenyl)ethylidene]hydrazine

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:460.3°Cat760mmHg
Flash Point:232.2°C
Density:1.29g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:326.10150494
Heavy Atom Count:24
Complexity:487

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NN=C(C)C1=CC(=CC=C1)[N+](=O)[O-])C2=CC(=CC=C2)[N+](=O)[O-]
Isomeric SMILES:C/C(=N\N=C(\C1=CC(=CC=C1)[N+](=O)[O-])/C)/C2=CC(=CC=C2)[N+](=O)[O-]

Technology Process of Bis[1-(3-nitrophenyl)ethylidene]hydrazine

There total 3 articles about Bis[1-(3-nitrophenyl)ethylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 121-89-1
3-Nitroacetophenone

: 5340-12-5
1,2-bis(1-(3-nitrophenyl)ethylidene)hydrazine

Guidance literature:: With carbazic acid; at 60 ℃; for 24h; Neat (no solvent);
DOI:10.1021/ol202593g

Reference yield:

: 22107-29-5
1-(3-nitro-phenyl)-ethanone semicarbazone

: 5340-12-5
1,2-bis(1-(3-nitrophenyl)ethylidene)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: silica gel / dichloromethane / Microwave irradiation

2: silica gel / dichloromethane / Microwave irradiation

With silica gel; In dichloromethane;
DOI:10.1080/00397911.2010.515334