3'-Adenylic acid, N-benzoyl-5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-O-(tetrahydro-2H -pyran-2-yl)-, 5-chloro-8-quinolinyl 2,6-dichlorophenyl ester

Base Information

• Chemical Name: 3'-Adenylic acid, N-benzoyl-5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-O-(tetrahydro-2H -pyran-2-yl)-, 5-chloro-8-quinolinyl 2,6-dichlorophenyl ester
• CAS No.: 116113-45-2
• Molecular Formula: C₅₈H₅₀Cl₃N₆O₁₁P
• Molecular Weight: 1144.4

Synonyms:

Chemical Property of 3'-Adenylic acid, N-benzoyl-5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-O-(tetrahydro-2H -pyran-2-yl)-, 5-chloro-8-quinolinyl 2,6-dichlorophenyl ester

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-Adenylic acid, N-benzoyl-5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-O-(tetrahydro-2H -pyran-2-yl)-, 5-chloro-8-quinolinyl 2,6-dichlorophenyl ester

There total 2 articles about 3'-Adenylic acid, N-benzoyl-5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-O-(tetrahydro-2H -pyran-2-yl)-, 5-chloro-8-quinolinyl 2,6-dichlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Chloro-8-hydroxyquinoline (130-16-5) → Phosphoric acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl ester 5-chloro-quinolin-8-yl ester 2,6-dichloro-phenyl ester (116113-45-2)

Guidance literature:

DOI:10.1016/S0040-4039(00)96821-7

Reference yield:

5'-O-(dimethoxytrityl)-2'-O-(tetrahydropyranyl)-N6-benzoyladenosine (71933-61-4) + 2,6-dichlorophenyl 5-chloro-8-quinolyl phosphorochloridate (93636-01-2) → Phosphoric acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl ester 5-chloro-quinolin-8-yl ester 2,6-dichloro-phenyl ester (116113-45-2)

Guidance literature:

Yield given;

DOI:10.1016/S0040-4039(00)96821-7

Reference yield:

Phosphoric acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl ester 5-chloro-quinolin-8-yl ester 2,6-dichloro-phenyl ester (116113-45-2) → Phosphoric acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl ester 5-chloro-quinolin-8-yl ester 2,6-dichloro-phenyl ester (116113-51-0)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; at 0 ℃; for 0.166667h;

DOI:10.1016/S0040-4039(00)96821-7

upstream raw materials:

5'-O-(dimethoxytrityl)-2'-O-(tetrahydropyranyl)-N⁶-benzoyladenosine

2,6-dichlorophenyl 5-chloro-8-quinolyl phosphorochloridate

5-Chloro-8-hydroxyquinoline

Downstream raw materials:

Phosphoric acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-4-(tetrahydro-pyran-2-yloxy)-tetrahydro-furan-3-yl ester 5-chloro-quinolin-8-yl ester 2,6-dichloro-phenyl ester

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