ISOMINTLACTONE

Base Information

Chemical Name:ISOMINTLACTONE
CAS No.:75684-66-1
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:
UNII:M282R422LI
DSSTox Substance ID:DTXSID30226599
Nikkaji Number:J11.289E
Mol file:75684-66-1.mol

Synonyms:(6R,7aS)-3,6-Dimethyl-5,6,7,7a-tetrahydro-4H-benzofuran-2-one;(+)-iso-mintlactone;(6R,7aS)-3,6-dimethyl-5,6,7,7a-tetrahydro-2(4H)-benzofuranone;(R)-isomintlactone;(+)-Isomintlactone;

Suppliers and Price of ISOMINTLACTONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of ISOMINTLACTONE

Chemical Property:

Melting Point:79-80 °C(Solv: ethyl ether (60-29-7); pentane (109-66-0))
Boiling Point:303.7±11.0 °C(Predicted)
PSA：26.30000
Density:1.07±0.1 g/cm3(Predicted)
LogP:2.04830
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:166.099379685
Heavy Atom Count:12
Complexity:253

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC2=C(C(=O)OC2C1)C
Isomeric SMILES:C[C@@H]1CCC2=C(C(=O)O[C@H]2C1)C

Technology Process of ISOMINTLACTONE

There total 53 articles about ISOMINTLACTONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 38049-03-5,77954-14-4,77965-62-9,79298-77-4,80924-17-0,82838-43-5,84709-83-1,121468-63-1,121468-69-7
(+/-)-6-methyl-3-methylene-hexahydrobenzofuran-2(3H)-one

: 13341-72-5,16434-36-9,16434-37-0,38049-04-6,51744-94-6,75684-66-1,142759-52-2,142759-53-3
(+/-) isomintlactone

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); In toluene; for 2h; Reflux;
DOI:10.1039/c1ob05709j

Reference yield: 68.0%

: 132060-11-8
2-(4-Methyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-propionic acid methyl ester

: 13341-72-5,16434-36-9,16434-37-0,38049-04-6,51744-94-6,75684-66-1,142759-52-2,142759-53-3
(+/-) isomintlactone

: 13341-72-5,16434-36-9,16434-37-0,38049-04-6,51744-94-6,75684-66-1,142759-52-2,142759-53-3
(+/-)-3,6-dimethyl-5,6,7,7a-tetrahydrobenzofuran-2(4H)-one

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; for 18h; Yield given. Title compound not separated from byproducts; Heating;
DOI:10.1016/S0040-4039(00)97172-7

Reference yield: 68.0%

: 132060-11-8
2-(4-Methyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-propionic acid methyl ester

: 13341-72-5,16434-36-9,16434-37-0,38049-04-6,51744-94-6,75684-66-1,142759-52-2,142759-53-3
(+/-) isomintlactone

: 13341-72-5,16434-36-9,16434-37-0,38049-04-6,51744-94-6,75684-66-1,142759-52-2,142759-53-3
(+/-)-3,6-dimethyl-5,6,7,7a-tetrahydrobenzofuran-2(4H)-one

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; for 18h; Yield given. Title compound not separated from byproducts; Heating;
DOI:10.1016/S0040-4039(00)97172-7