Benzoic acid,4-[1-(1,3-benzodioxol-5-yl)-2-[[[4-(1-methylethyl)phenyl]sulfonyl]amino]-2-oxoethoxy]-3-propyl-

Base Information

• Chemical Name: Benzoic acid,4-[1-(1,3-benzodioxol-5-yl)-2-[[[4-(1-methylethyl)phenyl]sulfonyl]amino]-2-oxoethoxy]-3-propyl-
• CAS No.: 159590-37-1
• Molecular Formula: C28H29 N O8 S
• Molecular Weight: 539.606
• Mol file: 159590-37-1.mol

Synonyms:L 749329

Chemical Property of Benzoic acid,4-[1-(1,3-benzodioxol-5-yl)-2-[[[4-(1-methylethyl)phenyl]sulfonyl]amino]-2-oxoethoxy]-3-propyl-

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid,4-[1-(1,3-benzodioxol-5-yl)-2-[[[4-(1-methylethyl)phenyl]sulfonyl]amino]-2-oxoethoxy]-3-propyl-

There total 2 articles about Benzoic acid,4-[1-(1,3-benzodioxol-5-yl)-2-[[[4-(1-methylethyl)phenyl]sulfonyl]amino]-2-oxoethoxy]-3-propyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

EtOAc-CH2 Cl2 + N-(4-iso-propylbenzenesulfonyl)-α-(4-carbomethoxy-2-n-propyl-phenoxy)-3,4-methylenedioxyphenylacetamide (159590-93-9) → N-[4-iso-propylbenzenesulfonyl]-2-(4-carboxy-2-propylphenoxy)-2-(3,4-methylenedioxyphenyl)acetamide (159590-37-1,173450-67-4)

Guidance literature:

With hydrogenchloride; potassium hydroxide; In methanol; water;

Reference yield: 91.0%

→ N-[4-iso-propylbenzenesulfonyl]-2-(4-carboxy-2-propylphenoxy)-2-(3,4-methylenedioxyphenyl)acetamide (159590-37-1,173450-67-4)

Guidance literature:

Reference yield:

2-amino-4,5-dihydro-1-methyl-1H-imidazol-4-one (creatinine) + CHCl3 -MeOH-concentrated NH4 OH + 1,1'-carbonyldiimidazole (530-62-1) + N-[4-iso-propylbenzenesulfonyl]-2-(4-carboxy-2-propylphenoxy)-2-(3,4-methylenedioxyphenyl)acetamide (159590-37-1,173450-67-4) → N-(4-isopropylbenzenesulfonyl)-α-[2-n-propyl-4-[[(4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)amino]carbonyl]phenoxy]-3,4-(methylenedioxy)phenylacetamide (178620-34-3)

Guidance literature:

With hydrogenchloride; triethylamine; In tetrahydrofuran; acetonitrile;

upstream raw materials:

N-(4-iso-propylbenzenesulfonyl)-α-(4-carbomethoxy-2-n-propyl-phenoxy)-3,4-methylenedioxyphenylacetamide

Downstream raw materials:

N-(4-iso-propylbenzenesulfonyl)-α-(4-(methylsulfonylcarbamyl)-2-n-propylphenoxy)-3,4-methylenedioxyphenylacetamide

N-(4-iso-propylbenzenesulfonyl)-α-(4-(sulfamylcarbamyl)-2-n-propylphenoxy)-3,4-methylenedioxyphenylacetamide

N-(4-isopropylbenzenesulfonyl)-α-[2-n-propyl-4-[[(4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)amino]carbonyl]phenoxy]-3,4-(methylenedioxy)phenylacetamide

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