11-Dodecenoic acid, 12-(triphenylgermyl)-, ethyl ester, (E)-

Base Information

Chemical Name:11-Dodecenoic acid, 12-(triphenylgermyl)-, ethyl ester, (E)-
CAS No.:116487-98-0
Molecular Formula:C32H40GeO2
Molecular Weight:529.258
Hs Code.:
Mol file:116487-98-0.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-Dodecenoic acid, 12-(triphenylgermyl)-, ethyl ester, (E)-

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Technology Process of 11-Dodecenoic acid, 12-(triphenylgermyl)-, ethyl ester, (E)-

There total 1 articles about 11-Dodecenoic acid, 12-(triphenylgermyl)-, ethyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2816-43-5
triphenylgermane

: 108545-41-1
11-dodecynoic acid ethyl ester

: 116487-98-0
(E)-ethyl 11-triphenylgermyl-10-undecenoate

Guidance literature:: triethyl borane; In hexane; benzene; addn. of Et3B in hexane to a soln. of acetylene-compd. and Ph3GeH in benzene, heating at 60°C for 15 h; purifn. by column chromy. or preparative thin-layer chromy. on silica gel,; elem. anal.; isomer ratio Z/E=<1/20 (detd. by GC, NMR);
DOI:10.1246/bcsj.63.2268