2-Bromo-3-(1-naphthyl)-1-propene

Base Information

• Chemical Name: 2-Bromo-3-(1-naphthyl)-1-propene
• CAS No.: 116545-04-1
• Molecular Formula: C13H11Br
• Molecular Weight: 247.13000
• DSSTox Substance ID: DTXSID30560208
• Wikidata: Q82443214
• Mol file: 116545-04-1.mol

Synonyms:2-BROMO-3-(1-NAPHTHYL)-1-PROPENE;116545-04-1;1-(2-bromoprop-2-enyl)naphthalene;1-(2-Bromoprop-2-en-1-yl)naphthalene;MFCD07775095;DTXSID30560208;AKOS016017293;Naphthalene, 1-(2-bromo-2-propen-1-yl)-

Chemical Property of 2-Bromo-3-(1-naphthyl)-1-propene

Chemical Property:

• Vapor Pressure: 0.000262mmHg at 25°C
• Boiling Point: 333.6oC at 760 mmHg
• Flash Point: 171.2oC
• PSA: 0.00000
• Density: 1.365g/cm3
• LogP: 4.29090
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 246.00441
• Heavy Atom Count: 14
• Complexity: 209

Purity/Quality:

97% ^*data from raw suppliers

2-BROMO-3-(1-NAPHTHYL)-1-PROPENE ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=C(CC1=CC=CC2=CC=CC=C21)Br

Technology Process of 2-Bromo-3-(1-naphthyl)-1-propene

There total 1 articles about 2-Bromo-3-(1-naphthyl)-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-naphthylmagnesiumbromide (703-55-9) + 2-bromoallyl bromide (513-31-5) → 1-(2-bromo-allyl)-naphthalene (116545-04-1)

Guidance literature:

With diethyl ether;

Reference yield: 89.0%

1-(2-bromo-allyl)-naphthalene (116545-04-1) → 1-(2-Iodo-allyl)-naphthalene (116545-00-7)

Guidance literature:

With copper(l) iodide; potassium iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 120 ℃; for 8h;

DOI:10.1055/s-1988-27527

upstream raw materials:

1-naphthylmagnesiumbromide

2-bromoallyl bromide

Downstream raw materials:

1-(2-Iodo-allyl)-naphthalene