Benzenemethanethiol, thallium(1+) salt

Base Information

Chemical Name:Benzenemethanethiol, thallium(1+) salt
CAS No.:117028-38-3
Molecular Formula:C₇H₇S*Tl
Molecular Weight:327.582
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanethiol, thallium(1+) salt

Chemical Property:

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Technology Process of Benzenemethanethiol, thallium(1+) salt

There total 2 articles about Benzenemethanethiol, thallium(1+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: thallium(I) carbonate

: 100-53-8
phenylmethanethiol

: 117028-38-3
phenylmethanethiolato thallium(I)

Guidance literature:: With N(C₂H₅)3; In acetonitrile; (under N2); to a suspn. of Tl2CO3 in acetonitrile was added a soln. of HSC7H7 and N(C2H5)3, mixt. was heated at reflux for several hours; pptn., filtn., filtrate was cooled at -20°C, pptn., recrystn. from acetonitrile, elem. anal.;

Reference yield:

: 20398-06-5
thallium (I) ethoxide

: 100-53-8
phenylmethanethiol

: 117028-38-3
phenylmethanethiolato thallium(I)

Guidance literature:: In pentane; slight excess of thiols; ppt. was dried in vac. for at least 3 h;
DOI:10.1021/ic0109243

Reference yield: 82.0%

: 117028-38-3
phenylmethanethiolato thallium(I)

: tris(2-mercapto-1-p-tolylimidazolyl)borate cadmium bromide

: [tris(2-mercapto-1-p-tolylimidazolyl)borate]CdSCH₂C₆H₅

Guidance literature:: In benzene; byproducts: TlBr; under N2, high vac. Schlenk technique; suspn. was stirred for 2 h; suspn. was filtered, solvent was removed from filtrate, ppt. was washed with pentane, dried in vac. for 1 h; elem. anal.;
DOI:10.1021/ic0109243