Magnesium bromide 4-methoxy-3-methylbenzen-1-ide (1/1/1)

Base Information

• Chemical Name: Magnesium bromide 4-methoxy-3-methylbenzen-1-ide (1/1/1)
• CAS No.: 117896-10-3
• Molecular Formula: C8H9BrMgO
• Molecular Weight: 225.368
• DSSTox Substance ID: DTXSID20452188
• Mol file: 117896-10-3.mol

Synonyms:Magnesium bromide 4-methoxy-3-methylbenzen-1-ide (1/1/1);magnesium;1-methoxy-2-methylbenzene-4-ide;bromide;117896-10-3;DTXSID20452188

Chemical Property of Magnesium bromide 4-methoxy-3-methylbenzen-1-ide (1/1/1)

Chemical Property:

• PSA: 9.23000
• LogP: 2.64940
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 223.96872
• Heavy Atom Count: 11
• Complexity: 185

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxy-3-methylphenylmagnesiumbromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=C[C-]=C1)OC.[Mg+2].[Br-]

Technology Process of Magnesium bromide 4-methoxy-3-methylbenzen-1-ide (1/1/1)

There total 1 articles about Magnesium bromide 4-methoxy-3-methylbenzen-1-ide (1/1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-4-bromoanisole (14804-31-0) → (4-methoxy-3-methylphenyl)magnesium bromide (117896-10-3)

Guidance literature:

With iodine; magnesium; In tetrahydrofuran; for 2h; Heating;

DOI:10.1039/b008319o

Reference yield: 99.0%

4-(methoxy-methyl-carbamoyl)-piperidine-1-carboxylic acid tert-butyl ester (370864-67-8) + (4-methoxy-3-methylphenyl)magnesium bromide (117896-10-3) → 4-(4-methoxy-3-methyl-benzoyl)-piperidine-1-carboxylic acid tert-butyl ester (1417917-64-6)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;

Reference yield: 86.0%

3-isobutoxy-5,5-dimethylcyclohex-2-en-1-one (15466-96-3) + (4-methoxy-3-methylphenyl)magnesium bromide (117896-10-3) → 4'-methoxy-3',5,5-trimethyl-5,6-dihydro-[1,1'-biphenyl]-3(4H)-one

Guidance literature:

3-isobutoxy-5,5-dimethylcyclohex-2-en-1-one; (4-methoxy-3-methylphenyl)magnesium bromide; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c9ob01373c

upstream raw materials:

2-methyl-4-bromoanisole

Downstream raw materials:

2-(3-methyl-4-methoxybenzoyl) benzoic acid

1,1,1-Trifluoro-2-(4-methoxy-3-methyl-phenyl)-propan-2-ol

3-methyl-4-methoxy-α,α,α-trifluoroacetophenone

(4-methoxy-3-methyl-phenyl)-acetone

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