(5E)-3-[4-({(E)-[(E)-[2-(4-chlorophenyl)hydrazinylidene](3,4-dimethoxyphenyl)methyl]diazenyl}carbonyl)phenyl]-5-(1H-indol-3-ylmethylidene)-2-methyl-3,5-dihydro-4H-imidazol-4-one

Base Information

Chemical Name:(5E)-3-[4-({(E)-[(E)-[2-(4-chlorophenyl)hydrazinylidene](3,4-dimethoxyphenyl)methyl]diazenyl}carbonyl)phenyl]-5-(1H-indol-3-ylmethylidene)-2-methyl-3,5-dihydro-4H-imidazol-4-one
CAS No.:134248-55-8
Molecular Formula:C₃₅H₂₈ClN₇O₄
Molecular Weight:646.105
Hs Code.:
Mol file:134248-55-8.mol

(5E)-3-[4-({(E)-[(E)-[2-(4-chlorophenyl)hydrazinylidene](3,4-dimethoxyphenyl)methyl]diazenyl}carbonyl)phenyl]-5-(1H-indol-3-ylmethylidene)-2-methyl-3,5-dihydro-4H-imidazol-4-one

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5E)-3-[4-({(E)-[(E)-[2-(4-chlorophenyl)hydrazinylidene](3,4-dimethoxyphenyl)methyl]diazenyl}carbonyl)phenyl]-5-(1H-indol-3-ylmethylidene)-2-methyl-3,5-dihydro-4H-imidazol-4-one

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:820.6°Cat760mmHg
Flash Point:450.1°C
Density:1.35g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (5E)-3-[4-({(E)-[(E)-[2-(4-chlorophenyl)hydrazinylidene](3,4-dimethoxyphenyl)methyl]diazenyl}carbonyl)phenyl]-5-(1H-indol-3-ylmethylidene)-2-methyl-3,5-dihydro-4H-imidazol-4-one

There total 5 articles about (5E)-3-[4-({(E)-[(E)-[2-(4-chlorophenyl)hydrazinylidene](3,4-dimethoxyphenyl)methyl]diazenyl}carbonyl)phenyl]-5-(1H-indol-3-ylmethylidene)-2-methyl-3,5-dihydro-4H-imidazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54753-57-0,70082-68-7,70082-69-8
4-(1'H-indol-3'-ylmethylene)-2-methyl-5(4H)oxazolone

: 134248-55-8
4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / 0.33 h / 140 °C

2: 75 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

3: 68 percent / glacial AcOH / ethanol / 5 h / Heating

4: 1) glacial AcOH, HCl, NaNO₂ 2) pyridine / 1) water, 0-5 deg C 2) r.t., overnight

With pyridine; hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 134248-29-6
Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

: 134248-55-8
4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

2: 68 percent / glacial AcOH / ethanol / 5 h / Heating

3: 1) glacial AcOH, HCl, NaNO₂ 2) pyridine / 1) water, 0-5 deg C 2) r.t., overnight

With pyridine; hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 134248-33-2
4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide

: 134248-55-8
4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / glacial AcOH / ethanol / 5 h / Heating

2: 1) glacial AcOH, HCl, NaNO₂ 2) pyridine / 1) water, 0-5 deg C 2) r.t., overnight

With pyridine; hydrogenchloride; acetic acid; sodium nitrite; In ethanol;