2-Thiophenesulfonamide, 4-[4-(bromomethyl)benzoyl]-

Base Information

Chemical Name:2-Thiophenesulfonamide, 4-[4-(bromomethyl)benzoyl]-
CAS No.:118993-69-4
Molecular Formula:C12H10BrNO3S2
Molecular Weight:360.24700
Hs Code.:
Mol file:118993-69-4.mol

Synonyms:4-(4-Bromomethylbenzoyl)-thiophene-2-sulfonamide;4-(4-bromomethylbenzoyl)thiophene-2-sulfonamide;4-(4-Bromomethyl-benzoyl)-thiophene-2-sulfonic acid amide;

Suppliers and Price of 2-Thiophenesulfonamide, 4-[4-(bromomethyl)benzoyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Thiophenesulfonamide, 4-[4-(bromomethyl)benzoyl]-

Chemical Property:

PSA：113.85000
LogP:4.30250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Thiophenesulfonamide, 4-[4-(bromomethyl)benzoyl]-

There total 5 articles about 2-Thiophenesulfonamide, 4-[4-(bromomethyl)benzoyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118993-68-3
4-<4-(bromomethyl)benzoyl>thiophene-2-sulfonyl chloride

: 118993-69-4
4-<4-(bromomethyl)benzoyl>thiophene-2-sulfonamide

Guidance literature:: With ammonia; In chloroform; at 0 - 10 ℃; for 3h; Yield given;
DOI:10.1021/jm00099a010

Reference yield:

: 118993-67-2
4-(4-Methylbenzoyl)-thiophene-2-sulfonyl chloride

: 118993-69-4
4-<4-(bromomethyl)benzoyl>thiophene-2-sulfonamide

Guidance literature:: With N-Bromosuccinimide; Perbenzoic acid; ammonia; Yield given. Multistep reaction; 1.) CHCl₃, reflux, irradiation, 0.5 h, 2.) 0 - 10 deg C, 3 h;
DOI:10.1002/jhet.5570260648

Reference yield:

: 118993-65-0
(thiophen-3-yl)(p-tolyl)methanone

: 118993-69-4
4-<4-(bromomethyl)benzoyl>thiophene-2-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / H₂SO₄, acetic anhydride / CH₂Cl₂ / 72 h / Ambient temperature

2: oxalyl chloride, N,N-dimethylformamide / ethyl acetate / 16 h / Ambient temperature

3: N-bromosuccinimide, benzoyl peroxide / CHCl₃ / 0.5 h / Heating; Irradiation

4: NH₃ (gas) / CHCl₃ / 3 h / 0 - 10 °C

With N-Bromosuccinimide; Perbenzoic acid; oxalyl dichloride; sulfuric acid; ammonia; acetic anhydride; N,N-dimethyl-formamide; In dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jm00099a010