1-Oxa-2-silacyclohex-3-ene, 2,2-dimethyl-6-phenyl-

Base Information

Chemical Name:1-Oxa-2-silacyclohex-3-ene, 2,2-dimethyl-6-phenyl-
CAS No.:119092-92-1
Molecular Formula:C12H16OSi
Molecular Weight:204.344
Hs Code.:
DSSTox Substance ID:DTXSID20464721
Nikkaji Number:J1.628.657E
Mol file:119092-92-1.mol

Synonyms:119092-92-1;1-Oxa-2-silacyclohex-3-ene, 2,2-dimethyl-6-phenyl-;SCHEMBL6435590;DTXSID20464721

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Oxa-2-silacyclohex-3-ene, 2,2-dimethyl-6-phenyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:204.097041664
Heavy Atom Count:14
Complexity:216

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si]1(C=CCC(O1)C2=CC=CC=C2)C

Technology Process of 1-Oxa-2-silacyclohex-3-ene, 2,2-dimethyl-6-phenyl-

There total 5 articles about 1-Oxa-2-silacyclohex-3-ene, 2,2-dimethyl-6-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 348597-89-7
dimethyl[(1-phenyl-3-butenyl)oxy]vinylsilane

: 119092-92-1
2,2-dimethyl-6-phenyl-1-oxa-2-silacyclohex-3-ene

Guidance literature:: bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum; In benzene; at 20 ℃; for 1h;
DOI:10.1021/ol015950j

Reference yield: 48.0%

: 119093-12-8
(3E)-4-[isopropoxy(dimethyl)silyl]-1-phenylbut-3-an-1-ol

: 119092-92-1
2,2-dimethyl-6-phenyl-1-oxa-2-silacyclohex-3-ene

Guidance literature:: In dichloromethane; at 20 ℃; for 26h; Irradiation;
DOI:10.1016/S0040-4020(01)86651-5

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 119092-92-1
2,2-dimethyl-6-phenyl-1-oxa-2-silacyclohex-3-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

2: 95 percent / [(CF₃)2C(Me)O]2Mo[CHCMe₂Ph][N-(2,6-diisopropylphenyl)] / benzene / 1 h / 20 °C

With triethylamine; bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum; In dichloromethane; benzene;
DOI:10.1016/j.tet.2004.06.149