2-(4-Methyl-3-nitrophenoxy)oxane

Base Information

Chemical Name:2-(4-Methyl-3-nitrophenoxy)oxane
CAS No.:119139-18-3
Molecular Formula:C12H15NO4
Molecular Weight:237.255
Hs Code.:
DSSTox Substance ID:DTXSID50555555

Synonyms:2-(4-Methyl-3-nitrophenoxy)oxane;119139-18-3;SCHEMBL3036505;DTXSID50555555;WQZUWDIDWUDELK-UHFFFAOYSA-N;2-(4-methyl-3-nitrophenoxy)tetrahydro-2H-pyran;2-(4-methyl-3-nitrophenoxy) tetrahydro-2H-pyran

Suppliers and Price of 2-(4-Methyl-3-nitrophenoxy)oxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(4-Methyl-3-nitrophenoxy)oxane

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:237.10010796
Heavy Atom Count:17
Complexity:266

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)OC2CCCCO2)[N+](=O)[O-]

Technology Process of 2-(4-Methyl-3-nitrophenoxy)oxane

There total 3 articles about 2-(4-Methyl-3-nitrophenoxy)oxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 2042-14-0
4-methyl-5-nitrophenol

: 119139-18-3
1-methyl-2-nitro-4-(tetrahydropyranyloxy)benzene

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 72h; Ambient temperature;
DOI:10.1016/S0040-4020(88)90025-7

Reference yield: 86.0%

: 694-54-2
tetrahydro-2H-2-pyranol

: 2042-14-0
4-methyl-5-nitrophenol

: 119139-18-3
1-methyl-2-nitro-4-(tetrahydropyranyloxy)benzene

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1055/s-2005-918916

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 119139-18-3
1-methyl-2-nitro-4-(tetrahydropyranyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / 2 h / 0 °C

2: 86 percent / PPh₃; diethylazodicarboxylate / tetrahydrofuran / 2 h / 20 °C

With hydrogenchloride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1055/s-2005-918916