2',3'-Dideoxy-2',3'-diazidoadenosine

Base Information

Chemical Name:2',3'-Dideoxy-2',3'-diazidoadenosine
CAS No.:119644-21-2
Molecular Formula:C10H11N11O2
Molecular Weight:317.26700
Hs Code.:
Mol file:119644-21-2.mol

Synonyms:2',3'-diazido-2',3'-dideoxyadenosine;[(2S,3S,4R,5R)-5-(6-Amino-purin-9-yl)-3,4-diazido-tetrahydro-furan-2-yl]-methanol;

Suppliers and Price of 2',3'-Dideoxy-2',3'-diazidoadenosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2',3'-Dideoxy-2',3'-diazidoadenosine

Chemical Property:

PSA：198.58000
LogP:0.14272

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2',3'-Dideoxy-2',3'-diazidoadenosine

There total 6 articles about 2',3'-Dideoxy-2',3'-diazidoadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 132980-97-3
9-<5-O-(tert-Butyldimethylsilyl)-2,3-diazido-2,3-dideoxy-β-D-ribofuranosyl>adenine

: 119644-21-2
9-(2,3-Diazido-2,3-dideoxy-β-D-ribofuranosyl)adenine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1h;
DOI:10.1021/jo00010a042

Reference yield:

: 132980-95-1
9-<3-Azido-5-O-(tert-butyldimethylsilyl)-3-deoxy-β-D-arabinofuranosyl>adenine

: 119644-21-2
9-(2,3-Diazido-2,3-dideoxy-β-D-ribofuranosyl)adenine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 0.17 h / 0 °C

2: 93 percent / LiN₃ / dimethylformamide / 0.75 h

3: 87 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h

With dmap; lithium azide; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00010a042

Reference yield:

: 132980-96-2
9-<3-Azido-5-O-(tert-butyldimethylsilyl)-3-deoxy-2-O-(trifluoromethanesulfonyl)-β-D-arabinofuranosyl>adenine

: 119644-21-2
9-(2,3-Diazido-2,3-dideoxy-β-D-ribofuranosyl)adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / LiN₃ / dimethylformamide / 0.75 h

2: 87 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h

With lithium azide; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00010a042