3H-1,2,4-Triazole-3-thione, 2,4-dihydro-4-(4-methylphenyl)-5-[[(3-phenylisoxazolo[5,4-d]pyrimidin-4- yl)oxy]methyl]-

Base Information

Chemical Name:3H-1,2,4-Triazole-3-thione, 2,4-dihydro-4-(4-methylphenyl)-5-[[(3-phenylisoxazolo[5,4-d]pyrimidin-4- yl)oxy]methyl]-
CAS No.:119898-35-0
Molecular Formula:C₂₁H₁₆N₆O₂S
Molecular Weight:416.463
Hs Code.:
Mol file:119898-35-0.mol

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Chemical Property of 3H-1,2,4-Triazole-3-thione, 2,4-dihydro-4-(4-methylphenyl)-5-[[(3-phenylisoxazolo[5,4-d]pyrimidin-4- yl)oxy]methyl]-

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Technology Process of 3H-1,2,4-Triazole-3-thione, 2,4-dihydro-4-(4-methylphenyl)-5-[[(3-phenylisoxazolo[5,4-d]pyrimidin-4- yl)oxy]methyl]-

There total 4 articles about 3H-1,2,4-Triazole-3-thione, 2,4-dihydro-4-(4-methylphenyl)-5-[[(3-phenylisoxazolo[5,4-d]pyrimidin-4- yl)oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 119898-17-8
C₂₁H₁₈N₆O₃S

: 119898-35-0
5-(3-Phenyl-isoxazolo[5,4-d]pyrimidin-4-yloxymethyl)-4-p-tolyl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: With sodium hydroxide; for 1h; Heating;

Reference yield:

: 119898-14-5
(3-Phenyl-isoxazolo[5,4-d]pyrimidin-4-yloxy)-acetic acid hydrazide

: 119898-35-0
5-(3-Phenyl-isoxazolo[5,4-d]pyrimidin-4-yloxymethyl)-4-p-tolyl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / aq. ethanol / 2 h / Heating

2: 68 percent / aq. NaOH / 1 h / Heating

With sodium hydroxide; In ethanol;

Reference yield:

: 119898-11-2
ethyl [(3-phenyl-4,5-dihydroisoxazolo[5,4-d]pyrimidin-4-yl)oxy]acetate

: 119898-35-0
5-(3-Phenyl-isoxazolo[5,4-d]pyrimidin-4-yloxymethyl)-4-p-tolyl-4H-[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / hydrazine hydrate / ethanol / 1.5 h / Heating

2: 74 percent / aq. ethanol / 2 h / Heating

3: 68 percent / aq. NaOH / 1 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;