1,8-dimethyl-9H-fluorene

Base Information

Chemical Name:1,8-dimethyl-9H-fluorene
CAS No.:1207-11-0
Molecular Formula:C15H14
Molecular Weight:194.27200
Hs Code.:2902909090
DSSTox Substance ID:DTXSID80399585
Nikkaji Number:J257.906E
Wikidata:Q82202228
Mol file:1207-11-0.mol

Synonyms:1,8-dimethyl-9H-fluorene;1207-11-0;9H-Fluorene, 1,8-dimethyl-;DTXSID80399585;AKOS024331421

Suppliers and Price of 1,8-dimethyl-9H-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,8-DIMETHYL-9H-FLUORENE 95.00%
5MG
$ 504.42

Total 9 raw suppliers

Chemical Property of 1,8-dimethyl-9H-fluorene

Chemical Property:

Melting Point:152-154 °C(Solv: methanol (67-56-1))
Boiling Point:332.4±22.0 °C(Predicted)
PSA：0.00000
Density:1.074±0.06 g/cm3(Predicted)
LogP:3.87460
XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:194.109550447
Heavy Atom Count:15
Complexity:208

Purity/Quality:

97% ^*data from raw suppliers

1,8-DIMETHYL-9H-FLUORENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2CC3=C(C=CC=C3C2=CC=C1)C

Technology Process of 1,8-dimethyl-9H-fluorene

There total 10 articles about 1,8-dimethyl-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 147644-47-1
3,6-Di-tert-butyl-1,8-dimethyl-9H-fluorene

: 1207-11-0
1,8-Dimethylfluoren

Guidance literature:: With aluminium trichloride; nitromethane; In benzene; at 50 ℃; for 4h;
DOI:10.1055/s-1993-25829

Reference yield:

: 58775-07-8
3,6-di-tert-butyl-9H-fluorene

: 1207-11-0
1,8-Dimethylfluoren

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / TiCl₄ / CS₂ / 5 h / 50 °C

2: 41 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

3: 25 percent / AlCl₃, MeNO₂ / benzene / 4 h / 50 °C

With lithium aluminium tetrahydride; aluminium trichloride; nitromethane; titanium tetrachloride; In tetrahydrofuran; carbon disulfide; benzene;
DOI:10.1055/s-1993-25829