4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide

Base Information

Chemical Name:4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide
CAS No.:1216-38-2
Molecular Formula:C15H21OPS
Molecular Weight:280.371
Hs Code.:
DSSTox Substance ID:DTXSID90405303
Wikidata:Q82209786

Synonyms:1216-38-2;4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide;DTXSID90405303;AKOS024325632;2,2,6,6-Tetramethyl-1-phenyl-1-thioxo-1I>>5-phosphinan-4-one;2,2,6,6-TETRAMETHYL-1-PHENYL-1-THIOXO-PHOSPHINAN-4-ONE

Suppliers and Price of 4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:280.10507346
Heavy Atom Count:18
Complexity:367

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(=O)CC(P1(=S)C2=CC=CC=C2)(C)C)C

Technology Process of 4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide

There total 3 articles about 4-Phosphorinanone, 2,2,6,6-tetramethyl-1-phenyl-, 1-sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

: 13887-05-3
1-phenyl-2,2,6,6-tetramethyl-4-phosphorinanone

: 1216-38-2
2,2,6,6-tetramethyl-1-phenyl-4-phosphorinanone 1-sulfide

Guidance literature:: With sulfur; In benzene; for 3h; Heating;
DOI:10.1021/jo00319a023

Reference yield:

: 504-20-1
phorone

: 1216-38-2
2,2,6,6-tetramethyl-1-phenyl-4-phosphorinanone 1-sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 72.5 percent / 6 h / 120 °C

2: 70.5 percent / S / benzene / 3 h / Heating

With sulfur; In benzene;
DOI:10.1021/jo00319a023

Reference yield:

: 638-21-1
phenylphosphane

: 1216-38-2
2,2,6,6-tetramethyl-1-phenyl-4-phosphorinanone 1-sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 72.5 percent / 6 h / 120 °C

2: 70.5 percent / S / benzene / 3 h / Heating

With sulfur; In benzene;
DOI:10.1021/jo00319a023