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4-allyl-4-ethylcyclohex-2-enone

Base Information Edit
  • Chemical Name:4-allyl-4-ethylcyclohex-2-enone
  • CAS No.:122444-62-6
  • Molecular Formula:C11H16O
  • Molecular Weight:164.247
  • Hs Code.:
  • Mol file:122444-62-6.mol
4-allyl-4-ethylcyclohex-2-enone

Synonyms:4-allyl-4-ethylcyclohex-2-enone;2-Cyclohexen-1-one,4-ethyl-4-(2-propenyl)-,(R);

Suppliers and Price of 4-allyl-4-ethylcyclohex-2-enone
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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  • Chemicals and raw materials
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Total 1 raw suppliers
Chemical Property of 4-allyl-4-ethylcyclohex-2-enone Edit
Chemical Property:
  • Boiling Point:237.2±10.0 °C(Predicted) 
  • PSA:17.07000 
  • Density:0.905±0.06 g/cm3(Predicted) 
  • LogP:2.87800 
Purity/Quality:

99% *data from raw suppliers

Safty Information:
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MSDS Files:
Useful:
Technology Process of 4-allyl-4-ethylcyclohex-2-enone

There total 5 articles about 4-allyl-4-ethylcyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.67 h / Inert atmosphere; Cooling with ice
1.2: 1.58 h / Inert atmosphere; Cooling with acetone-dry ice; Cooling with ice
2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / -80 - 0 °C / Inert atmosphere
3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / Cooling with acetone-dry ice; Inert atmosphere
3.2: 24 h / Reflux; Inert atmosphere
With sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; toluene;
DOI:10.15227/orgsyn.069.0055
Guidance literature:
Multi-step reaction with 4 steps
1.1: toluene / 18 h / Reflux; Inert atmosphere
2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.67 h / Inert atmosphere; Cooling with ice
2.2: 1.58 h / Inert atmosphere; Cooling with acetone-dry ice; Cooling with ice
3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / -80 - 0 °C / Inert atmosphere
4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / Cooling with acetone-dry ice; Inert atmosphere
4.2: 24 h / Reflux; Inert atmosphere
With sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; toluene;
DOI:10.15227/orgsyn.069.0055
Guidance literature:
With tetrabutylammonium dihydrogen phosphate; sodium bis(2-methoxyethoxy)aluminium dihydride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) toluene, RT, 3 d, 2.) ethanol, reflux, 24 h;
DOI:10.1021/jo00280a040
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