Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy-

Base Information

Chemical Name:Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy-
CAS No.:124609-17-2
Molecular Formula:C16H20O3
Molecular Weight:260.333
Hs Code.:
DSSTox Substance ID:DTXSID90450994
Mol file:124609-17-2.mol

Synonyms:124609-17-2;Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy-;SCHEMBL8888962;DTXSID90450994

Suppliers and Price of Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy-

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:260.14124450
Heavy Atom Count:19
Complexity:310

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1CC2=CCCCC2)OC)C=O

Technology Process of Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy-

There total 7 articles about Benzaldehyde, 4-(1-cyclohexen-1-ylmethyl)-3,5-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 144337-58-6
4-(1'-cyclohexenyl)methyl-3,5-dimethoxybenzyl alcohol

: 124609-17-2
4-(cyclohex-1-en-1-ylmethyl)-3,5-dimethoxybenzaldehyde

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane;

Reference yield: 70.0%

: 124609-16-1
4-(cyclohexylhydroxymethyl)-3,5-dimethoxybenzaldehyde

: 124609-17-2
4-(cyclohex-1-en-1-ylmethyl)-3,5-dimethoxybenzaldehyde

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 24h; Heating;

Reference yield:

: 59276-34-5
3,5-dimethoxybenzaldehyde dimethyl acetal

: 124609-17-2
4-(cyclohex-1-en-1-ylmethyl)-3,5-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: TMEDA; n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

1.2: CuI / tetrahydrofuran; hexane / -70 - -45 °C

1.3: tetrahydrofuran; hexane / 24 h / 20 °C

2.1: 870 mg / aq. HCl / diethyl ether / 16 h

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jm0204284