2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide

Base Information

Chemical Name:2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide
CAS No.:126299-26-1
Molecular Formula:C₁₆H₁₅N₃O₃
Molecular Weight:297.313
Hs Code.:
DSSTox Substance ID:DTXSID00560270
Mol file:126299-26-1.mol

Synonyms:126299-26-1;DTXSID00560270;2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide

Suppliers and Price of 2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:297.11134135
Heavy Atom Count:22
Complexity:419

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C(C(=O)NC1=CC=CC=C1)N=NC2=CC(=CC=C2)O

Technology Process of 2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide

There total 2 articles about 2-[(E)-(3-Hydroxyphenyl)diazenyl]-3-oxo-N-phenylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 126299-26-1
3-(3-acetoacetanilido)-azo-1-hydroxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl, sodium nitrite / H₂O / 0 °C

2: 10percent NaOH / aq. ethanol

With hydrogenchloride; sodium hydroxide; sodium nitrite; In ethanol; water;

Reference yield:

: 17404-99-8
3-hydroxy-benzenediazonium; chloride

: 102-01-2,98624-45-4
N-phenylacetoacetamide

: 126299-26-1
3-(3-acetoacetanilido)-azo-1-hydroxybenzene

Guidance literature:: With sodium hydroxide; In ethanol; Yield given;

Reference yield:

: 126299-26-1
3-(3-acetoacetanilido)-azo-1-hydroxybenzene

: 10108-64-2
cadmium(II) chloride

: Cd⁽²⁺⁾*OC₆H₄NNC(C(O)CH₃)C(O)NHC₆H₅^(2-) = {Cd(OC₆H₄NNC(C(O)CH₃)C(O)NHC₆H₅)}

Guidance literature:: In 1,4-dioxane; ethanol; adding ethanolic sol. CdCl2 to the ligand dissolved in dioxane in 1:1 molar ratio; pH around 7; filtered; washed (ethanol; ether); dried under reduced pressure; elem. anal.;