1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol

Base Information

Chemical Name:1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol
CAS No.:127782-77-8
Molecular Formula:C₁₃H₂₀N₂O
Molecular Weight:220.315
Hs Code.:
DSSTox Substance ID:DTXSID10568585
Nikkaji Number:J282.209A
Wikidata:Q82454883
Mol file:127782-77-8.mol

Synonyms:127782-77-8;SCHEMBL9752146;DTXSID10568585;1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol

Suppliers and Price of 1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:220.157563266
Heavy Atom Count:16
Complexity:259

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C=CN=C1C(=C)CC2(CCCCC2)O

Technology Process of 1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol

There total 2 articles about 1-[2-(1-Methyl-1H-imidazol-2-yl)prop-2-en-1-yl]cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86354-06-5
2-(1-hydroxy-1-methylethyl)-1-methylimidazole

: 127782-77-8
2-<1-(1-hydroxycyclohexyl)-2-propen-2-yl>-1-methyl-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Ac₂O / acetic acid / 4 h / 130 - 140 °C

2: 1. Et₃Al, BuLi / 1. hexane, -78 deg C, HMPT, 15 min 2. -50 deg C, 15 min

With n-butyllithium; triethylaluminum; acetic anhydride; In acetic acid;
DOI:10.1055/s-1990-26794

Reference yield:

: 127782-73-4
2-(1-methylethenyl)-1-methylimidazole

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 127782-77-8
2-<1-(1-hydroxycyclohexyl)-2-propen-2-yl>-1-methyl-1H-imidazole

Guidance literature:: With n-butyllithium; triethylaluminum; Yield given. Multistep reaction; 1. hexane, -78 deg C, HMPT, 15 min 2. -50 deg C, 15 min;
DOI:10.1055/s-1990-26794