3-Cyclohexylprop-1-en-2-ylsulfonylbenzene

Base Information

Chemical Name:3-Cyclohexylprop-1-en-2-ylsulfonylbenzene
CAS No.:129855-21-6
Molecular Formula:C15H20O2S
Molecular Weight:264.389
Hs Code.:
DSSTox Substance ID:DTXSID70564048
Wikidata:Q82448627

Synonyms:3-cyclohexylprop-1-en-2-ylsulfonylbenzene;129855-21-6;DTXSID70564048;1-(cyclohexylmethyl)vinylsulfonylbenzene;(3-Cyclohexylprop-1-ene-2-sulfonyl)benzene

Suppliers and Price of 3-Cyclohexylprop-1-en-2-ylsulfonylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Cyclohexylprop-1-en-2-ylsulfonylbenzene

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:264.11840105
Heavy Atom Count:18
Complexity:366

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(CC1CCCCC1)S(=O)(=O)C2=CC=CC=C2

Technology Process of 3-Cyclohexylprop-1-en-2-ylsulfonylbenzene

There total 6 articles about 3-Cyclohexylprop-1-en-2-ylsulfonylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 110-82-7,25012-93-5
cyclohexane

: 2525-55-5
(prop-2-ene-1,2-diyldisulfonyl)dibenzene

: 129855-21-6
3-cyclohexyl-2-(phenylsulfonyl)-1-propene

Guidance literature:: With pentacene-5,7,12,14-tetraone; potassium carbonate; In dichloromethane; at 20 ℃; for 24h; chemoselective reaction; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.6b03586

Reference yield: 53.0%

: 108-85-0
1-bromocyclohexane

: 2525-55-5
(prop-2-ene-1,2-diyldisulfonyl)dibenzene

: 129855-21-6
3-cyclohexyl-2-(phenylsulfonyl)-1-propene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;
DOI:10.1021/jo00027a052

Reference yield:

: 2525-54-4
3-(phenylsulfonyl)-2-(phenylthio)-1-propene

: 129855-21-6
3-cyclohexyl-2-(phenylsulfonyl)-1-propene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / H₂O₂, glac.HOAc / 25 °C

2: 53 percent / n-Bu₃SnH, AIBN / benzene / Heating

With 2,2'-azobis(isobutyronitrile); dihydrogen peroxide; tri-n-butyl-tin hydride; acetic acid; In benzene;
DOI:10.1021/jo00027a052