Technology Process of Benzene, [(3-methylpentadecyl)sulfonyl]-, (S)-
There total 5 articles about Benzene, [(3-methylpentadecyl)sulfonyl]-, (S)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 12h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) diphenyl diselenide, 35 percent hydrogen peroxide, 2.) tert-butyl hydroperoxide / 1.) methylene chloride, r.t., 6 h, 2.) r.t., 20 h
2: 1.) ozone, 2.) sodium borohydride / 1.) chloroform, -20 deg C, 2.) ethanol, water, heating, 2 h
3: 96 percent / pyridine / 12 h / 0 - 5 °C
4: 1.) sodium hydroxide / 1.) methanol, r.t., 1 h, 2.) reflux, 12 h
5: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 12 h / Ambient temperature
With
pyridine; tert.-butylhydroperoxide; sodium hydroxide; sodium tetrahydroborate; diphenyl diselenide; dihydrogen peroxide; ozone; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) ozone, 2.) sodium borohydride / 1.) chloroform, -20 deg C, 2.) ethanol, water, heating, 2 h
2: 96 percent / pyridine / 12 h / 0 - 5 °C
3: 1.) sodium hydroxide / 1.) methanol, r.t., 1 h, 2.) reflux, 12 h
4: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 12 h / Ambient temperature
With
pyridine; sodium hydroxide; sodium tetrahydroborate; ozone; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;