9-Octadecen-11-ynoic acid, (9Z)-

Base Information

Chemical Name:9-Octadecen-11-ynoic acid, (9Z)-
CAS No.:13089-74-2
Molecular Formula:C18H30O2
Molecular Weight:
Hs Code.:

Synonyms:

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Chemical Property of 9-Octadecen-11-ynoic acid, (9Z)-

Chemical Property:

Purity/Quality:

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Technology Process of 9-Octadecen-11-ynoic acid, (9Z)-

There total 6 articles about 9-Octadecen-11-ynoic acid, (9Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 913971-71-8
(Z)-methyl octadec-9-en-11-ynoate

: 13089-74-2
(Z)-octadec-9-en-11-ynoic acid

Guidance literature:: (Z)-methyl octadec-9-en-11-ynoate; With methanol; sodium hydroxide; water; at 23 ℃; for 7h;

With hydrogenchloride; In water; pH=2;

Reference yield: 86.0%

: octadec-9-en-11-ynoic acid tert-butyl ester

: 13089-74-2
(Z)-octadec-9-en-11-ynoic acid

Guidance literature:: With cerium(III) chloride; sodium iodide; In acetonitrile; for 5h; Heating;
DOI:10.1021/jo010010y

Reference yield:

: 112-62-9
Methyl oleate

: 13089-74-2
(Z)-octadec-9-en-11-ynoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: ozone / dichloromethane / -78 °C

1.2: 18 h / -78 - 23 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.17 h / 23 °C

2.2: 2.58 h / -78 - 23 °C

3.1: triethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / acetonitrile / 22 h / -20 - 23 °C

4.1: methanol; sodium hydroxide; water / 7 h / 23 °C

4.2: pH 2

With methanol; sodium hydroxide; water; sodium hexamethyldisilazane; ozone; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; dichloromethane; acetonitrile;