Benzaldehyde, 4-(dipropylamino)-2-methoxy-

Base Information

Chemical Name:Benzaldehyde, 4-(dipropylamino)-2-methoxy-
CAS No.:131190-89-1
Molecular Formula:C14H21NO2
Molecular Weight:235.326
Hs Code.:

Synonyms:

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Chemical Property of Benzaldehyde, 4-(dipropylamino)-2-methoxy-

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Technology Process of Benzaldehyde, 4-(dipropylamino)-2-methoxy-

There total 4 articles about Benzaldehyde, 4-(dipropylamino)-2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35666-61-6
2-methoxy-N,N-dipropylaniline

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 131190-89-1
C₁₄H₂₁NO₂

Guidance literature:: N,N-dimethyl-formamide; With phosphorus trichloride; at -10 - 0 ℃; for 0.333333h;

2-methoxy-N,N-dipropylaniline; In N,N-dimethyl-formamide; at 110 ℃; for 2h;

With water; sodium hydrogencarbonate; In N,N-dimethyl-formamide;

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 131190-89-1
C₁₄H₂₁NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; sodium stearate; tetrabutylammomium bromide / water; ethanol / 100 °C

2: trichlorophosphate / 0 - 80 °C

With tetrabutylammomium bromide; sodium stearate; potassium carbonate; trichlorophosphate; In ethanol; water; 2: |Vilsmeier-Haack Formylation / 2: |Vilsmeier-Haack Formylation;
DOI:10.1021/acsmedchemlett.5b00049

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 131190-89-1
C₁₄H₂₁NO₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / isopropyl alcohol; water / 8 h / 70 °C

2: trichlorophosphate / Combinatorial reaction / High throughput screening (HTS); Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 8 h / Heating

With sodium carbonate; potassium carbonate; trichlorophosphate; In water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.dyepig.2016.08.043