Benzene, 1-(2-bromoethenyl)-4-nitro-

Base Information

Chemical Name:Benzene, 1-(2-bromoethenyl)-4-nitro-
CAS No.:13161-29-0
Molecular Formula:C8H6BrNO2
Molecular Weight:228.045
Hs Code.:
European Community (EC) Number:654-715-3
DSSTox Substance ID:DTXSID40405474

Synonyms:Benzene, 1-(2-bromoethenyl)-4-nitro-;1-(2-bromoethenyl)-4-nitrobenzene;13161-29-0;1-(2-BROMO-VINYL)-4-NITRO-BENZENE;DTXSID40405474;AB04153

Suppliers and Price of Benzene, 1-(2-bromoethenyl)-4-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzene, 1-(2-bromoethenyl)-4-nitro-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:226.95819
Heavy Atom Count:12
Complexity:180

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C=CBr)[N+](=O)[O-]

Technology Process of Benzene, 1-(2-bromoethenyl)-4-nitro-

There total 7 articles about Benzene, 1-(2-bromoethenyl)-4-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 619-89-6
p-nitrocinnamic acid

: 13161-29-0
p-nitrocinnamyl bromide

Guidance literature:: With [bis(acetoxy)iodo]benzene; tetraethylammonium bromide; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1248/cpb.57.1243

Reference yield:

: 35447-78-0
2,3-dibromo-3-(4-nitro-phenyl)-propionic acid

: 13161-29-0
p-nitrocinnamyl bromide

Guidance literature:: With ethanol; sodium acetate; lower-melting form;
DOI:10.1002/hlca.19200030122

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 13161-29-0
p-nitrocinnamyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; piperidine / isopropyl alcohol / Heating

2: bromine; acetic acid / dichloromethane / 20 °C

3: triethylamine / N,N-dimethyl-formamide / 0.03 h / 35 °C / Microwave irradiation

With piperidine; pyridine; bromine; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; 1: |Knoevenagel-Doebner-Stobbe Reaction;
DOI:10.1016/j.ejmech.2019.03.047