2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid

Base Information

Chemical Name:2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid
CAS No.:131933-37-4
Molecular Formula:C22H18O6
Molecular Weight:378.381
Hs Code.:
DSSTox Substance ID:DTXSID80548839
Nikkaji Number:J1.509.487G
Wikidata:Q82427675

Synonyms:131933-37-4;2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid;SCHEMBL3424839;DTXSID80548839;MNGZHXUINUBLGV-UHFFFAOYSA-N;2,3-Bis(benzyloxy)terephthalic acid

Suppliers and Price of 2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:378.11033829
Heavy Atom Count:28
Complexity:463

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C=CC(=C2OCC3=CC=CC=C3)C(=O)O)C(=O)O

Technology Process of 2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid

There total 6 articles about 2,3-Bis(benzyloxy)benzene-1,4-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2,3-bis(benzyloxy)terephthalic acid dibenzyl ester

: 131933-37-4
2,3-bis(benzyloxy)-terephthalic acid

Guidance literature:: 2,3-bis(benzyloxy)terephthalic acid dibenzyl ester; With lithium hydroxide; In 1,4-dioxane; ethanol; water; at 60 ℃; for 12h;

With hydrogenchloride; In water;

Reference yield: 94.0%

: 131851-93-9
dimethyl 2,3-bis(benzyloxy)terephthalate

: 131933-37-4
2,3-bis(benzyloxy)-terephthalic acid

Guidance literature:: With sodium hydroxide; In 1,2-dimethoxyethane; for 9h; Heating;

Reference yield:

: 75956-62-6
dimethyl 2,3-dihydroxyterephthalate

: 131933-37-4
2,3-bis(benzyloxy)-terephthalic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / KI, K₂CO₃ / acetone / 96 h / Heating

2: 94 percent / 3.3 M aq. NaOH / 1,2-dimethoxy-ethane / 9 h / Heating

With sodium hydroxide; potassium carbonate; potassium iodide; In 1,2-dimethoxyethane; acetone;