2-Methoxy-1-[(2-methoxynaphthalen-1-yl)methyl]naphthalene

Base Information

• Chemical Name: 2-Methoxy-1-[(2-methoxynaphthalen-1-yl)methyl]naphthalene
• CAS No.: 2212-45-5
• Molecular Formula: C23H20 O2
• Molecular Weight: 328.411
• NSC Number: 51645
• DSSTox Substance ID: DTXSID60176639
• Mol file: 2212-45-5.mol

Synonyms:2212-45-5;2-methoxy-1-[(2-methoxynaphthalen-1-yl)methyl]naphthalene;Naphthalene, 1,1'-methylenebis(2-methoxy-;Bis(2-methoxynaphthalen-1-yl)methane;NSC51645;BRN 2301044;1,1'-Methylenebis(2-methoxynaphthalene);starbld0027046;SCHEMBL19766698;DTXSID60176639;NSC 51645;NSC-51645

Chemical Property of 2-Methoxy-1-[(2-methoxynaphthalen-1-yl)methyl]naphthalene

Chemical Property:

• Boiling Point: 498.3°Cat760mmHg
• Flash Point: 193.7°C
• Density: 1.151g/cm³
• XLogP3: 6.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 328.146329876
• Heavy Atom Count: 25
• Complexity: 384

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C2=CC=CC=C2C=C1)CC3=C(C=CC4=CC=CC=C43)OC

Technology Process of 2-Methoxy-1-[(2-methoxynaphthalen-1-yl)methyl]naphthalene

There total 1 articles about 2-Methoxy-1-[(2-methoxynaphthalen-1-yl)methyl]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(2-hydroxy-1-naphthyl)methane (1096-84-0) + dimethyl sulfate (77-78-1) → monomethyl ester of bis(2-hydroxy-1-naphthyl)methane (33230-77-2) + Bis(2-methoxynaphthalen-1-yl)methane (2212-45-5)

Guidance literature:

With potassium hydroxide; acetone;

DOI:10.1080/00220670209598791

Reference yield: 75.0%

Bis(2-methoxynaphthalen-1-yl)methane (2212-45-5) → bis(2-hydroxy-1-naphthyl)methane (1096-84-0)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + Bis(2-methoxynaphthalen-1-yl)methane (2212-45-5) + acetic acid (64-19-7,77671-22-8) → 2-Methoxynaphthalene (93-04-9)

Guidance literature:

DOI:10.1021/jo01232a005

upstream raw materials:

bis(2-hydroxy-1-naphthyl)methane

dimethyl sulfate

Downstream raw materials:

(2-acetoxy-[1]naphthyl)-(2-methoxy-[1]naphthyl)-methane

2-Methoxynaphthalene

monomethyl ester of bis(2-hydroxy-1-naphthyl)methane

bis(2-hydroxy-1-naphthyl)methane

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