4-[(4-CHLOROBENZYL)OXY]BENZALDEHYDE

Base Information

• Chemical Name: 4-[(4-CHLOROBENZYL)OXY]BENZALDEHYDE
• CAS No.: 59067-46-8
• Molecular Formula: C14H11ClO2
• Molecular Weight: 246.693
• Hs Code.: 2913000090
• Mol file: 59067-46-8.mol

Synonyms:4-(4-Chlorobenzyloxy)benzaldehyde;4-[(4-Chlorophenyl)methoxy]benzaldehyde;

Chemical Property of 4-[(4-CHLOROBENZYL)OXY]BENZALDEHYDE

Chemical Property:

• Vapor Pressure: 2.07E-06mmHg at 25°C
• Refractive Index: 1.615
• Boiling Point: 393.9 °C at 760 mmHg
• Flash Point: 164.7 °C
• PSA: 26.30000
• Density: 1.247 g/cm³
• LogP: 3.73150
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

4-[(4-Chlorobenzyl)oxy]benzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[(4-CHLOROBENZYL)OXY]BENZALDEHYDE

There total 7 articles about 4-[(4-CHLOROBENZYL)OXY]BENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.2%

4-chlorobenzyl bromide (622-95-7) + 4-hydroxy-benzoic acid (99-96-7) → 4-[(4-chlorobenzyl)oxy]benzaldehyde (59067-46-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;

Reference yield: 89.0%

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) + 1-Chloro-4-(chloromethyl)benzene (104-83-6) → 4-[(4-chlorobenzyl)oxy]benzaldehyde (59067-46-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1002/asia.201100154

Reference yield: 88.0%

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-[(4-chlorobenzyl)oxy]benzaldehyde (59067-46-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Heating;

DOI:10.3390/molecules26195770

upstream raw materials:

4-hydroxy-benzaldehyde

1-Chloro-4-(chloromethyl)benzene

4-chlorobenzyl bromide

4-hydroxy-benzoic acid

Downstream raw materials:

ethyl 2-fluoro-3-<4-(4-chlorobenzyloxy)phenyl>acrylate

2-<4-(4-chlorobenzyloxy)phenyl>-2-hydroxyacetonitrile

4-(4-chlorobenzyloxy)benzyl alcohol

3-(4-hydroxy-phenyl)-propionic acid ethyl ester

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