2-(Bromoacetyl)pyridine hydrobromide

Base Information

• Chemical Name: 2-(Bromoacetyl)pyridine hydrobromide
• CAS No.: 17570-98-8
• Molecular Formula: C7H7Br2NO
• Molecular Weight: 280.947
• Hs Code.: 2933399090
• European Community (EC) Number: 642-647-7
• NSC Number: 73994
• DSSTox Substance ID: DTXSID40379909
• Mol file: 17570-98-8.mol

Synonyms:2-(Bromoacetyl)pyridine hydrobromide;17570-98-8;2-bromo-1-(pyridin-2-yl)ethanone hydrobromide;2-bromo-1-(2-pyridinyl)-1-ethanone hydrobromide;2-(2-bromoacetyl)pyridine hydrobromide;2-(BROMOACETYL)PYRIDINE HBR;2-bromo-1-pyridin-2-ylethanone;hydrobromide;MFCD02181196;2-BROMO-1-(PYRIDIN-2-YL)ETHAN-1-ONE HYDROBROMIDE;2-bromoacetylpyridine hydrobromide;hydron;bromide;2-Bromo-1-(2-pyridinyl)-1-ethanone hydrobromide;2-bromo-1-pyridin-2-ylethanone hydrobromide;Bromoacetylpyridine hydrobromide;SCHEMBL1016601;DTXSID40379909;BYKVUGZUYJUSKD-UHFFFAOYSA-N;2-(bromoacetyl)pyridinehydrobromide;NSC73994;(2-bromoacetyl)pyridine hydrobromide;NSC-73994;2-(bromoacetyl) pyridine hydrobromide;2-(bromoacetyl)-pyridine hydrobromide;AKOS007930886;CS-W004138;2-(2-Bromoethanoyl)pyridine hydrobromide;2-bromo-1-pyridin-ylethanone hydrobromide;AM803353;AS-18166;BP-12046;SY007962;2-bromo-1-pyrid-2-ylethanone hydrobromide;FT-0611330;2-bromo-1-(2-pyridinyl)ethanone hydrobromide;2-bromo-1-pyridin-2-yl ethanone hydrobromide;2-Bromo-1-pyridin-2-ylmethanone hydrobromide;2-bromo-1-(2-pyridinyl)-ethanone hydrobromide;EN300-205579;2-Bromo-1-(2-pyridinyl)1-ethanone hydrobromide;2-bromo-1-(2-pyridyl)ethan-1-one hydrobromide;2-bromo-1-(2-pyridyl)ethanone hydrobromide salt;2-bromo-1-(pyridin-2-yl)ethanone, hydrobromide;A812106;A824910;J-508138;Ethanone, 2-bromo-1-(2-pyridinyl)-, hydrobromide (1:1);2-bromo-1-(2-pyridinyl)-1-ethanone hydrobromide, AldrichCPR

Chemical Property of 2-(Bromoacetyl)pyridine hydrobromide

Chemical Property:

• Vapor Pressure: 0.0233mmHg at 25°C
• Melting Point: 205 °C
• Boiling Point: 249.1 °C at 760 mmHg
• Flash Point: 104.5 °C
• PSA: 29.96000
• Density: 1.57g/cm3
• LogP: 2.61730
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 280.88739
• Heavy Atom Count: 11
• Complexity: 127

Purity/Quality:

97% ^*data from raw suppliers

2-(Bromoacetyl)pyridinehydrobromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi,Xn
• Statements: 36/37/38-36-22
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=NC(=C1)C(=O)CBr.Br

Technology Process of 2-(Bromoacetyl)pyridine hydrobromide

There total 4 articles about 2-(Bromoacetyl)pyridine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.8%

2-acetylpyridine (1122-62-9) → 2-(bromoacetyl)pyridine hydrobromide (17570-98-8)

Guidance literature:

With hydrogen bromide; bromine; acetic acid; at 15 - 75 ℃; for 2h;

Reference yield: 90.0%

methyl (4-pyridyl) ketone (1122-54-9) → 2-(bromoacetyl)pyridine hydrobromide (17570-98-8)

Guidance literature:

With hydrogen bromide; bromine; acetic acid; In water; at 20 ℃;

Reference yield: 18.9%

2-acetylpyridinium bromide (113738-31-1) → 2-(bromoacetyl)pyridine hydrobromide (17570-98-8)

Guidance literature:

With bromine; In acetic acid; benzene; at 60 ℃;

DOI:10.1016/S0040-4020(01)90316-3

upstream raw materials:

2-acetylpyridine

2-acetylpyridinium bromide

methyl (4-pyridyl) ketone

Downstream raw materials:

2-oxo-2-(pyridin-2-yl)ethyl acetate

3-[1-Phenyl-meth-(Z)-ylidene]-6-pyridin-2-yl-[1,4]oxathiin-2-one

2-Hydrazino-4-(2'-pyridyl)thiazole

2-pyridacyl benzoate