Diazenecarboxamide, 2-(2,4,6-trichlorophenyl)-

Base Information

Chemical Name:Diazenecarboxamide, 2-(2,4,6-trichlorophenyl)-
CAS No.:133546-58-4
Molecular Formula:C7H4Cl3N3O
Molecular Weight:252.487
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diazenecarboxamide, 2-(2,4,6-trichlorophenyl)-

Chemical Property:

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Technology Process of Diazenecarboxamide, 2-(2,4,6-trichlorophenyl)-

There total 1 articles about Diazenecarboxamide, 2-(2,4,6-trichlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 133546-57-3
2,4,6-trichlorophenylsemicarbazide

: 133546-58-4
2,4,6-trichlorophenylazocarboxamide

Guidance literature:: With Pb(OAc)3; In dichloromethane; for 10h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89022-0

Reference yield: 89.0%

: 133546-58-4
2,4,6-trichlorophenylazocarboxamide

: 58468-74-9
2,4,6-trichlorobenzenediazocyanide

Guidance literature:: With pyridine; trifluoroacetic anhydride; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89022-0

Reference yield:

: 133546-58-4
2,4,6-trichlorophenylazocarboxamide

: 143262-38-8
3-(2,4,6-Trichloro-phenyl)-2,3-diaza-bicyclo[2.2.1]hept-5-ene-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / trifluoroacetic anhydride, pyridine / tetrahydrofuran / 3 h / Ambient temperature

2: 85 percent / CH₂Cl₂

With pyridine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)89022-0