Akuammilan-17-oic acid, 1,2-dihydro-10-hydroxy-1-methyl-, methyl ester, (2beta)-

Base Information

• Chemical Name: Akuammilan-17-oic acid, 1,2-dihydro-10-hydroxy-1-methyl-, methyl ester, (2beta)-
• CAS No.: 81827-54-5
• Molecular Formula: C₂₁H₂₆N₂O₃
• Molecular Weight: 354.449
• Mol file: 81827-54-5.mol

Synonyms:Akuammilan-17-oic acid, 1,2-dihydro-10-hydroxy-1-methyl-, methyl ester, (2beta)-;81827-54-5

Chemical Property of Akuammilan-17-oic acid, 1,2-dihydro-10-hydroxy-1-methyl-, methyl ester, (2beta)-

Chemical Property:

• Vapor Pressure: 5.36E-12mmHg at 25°C
• Boiling Point: 533.5°Cat760mmHg
• Flash Point: 276.5°C
• Density: 1.31g/cm³
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 354.19434270
• Heavy Atom Count: 26
• Complexity: 649

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC=C1CN2CCC34C(C1CC2C3N(C5=C4C=C(C=C5)O)C)C(=O)OC
• Isomeric SMILES: C/C=C\1/CN2CCC34C(C1CC2C3N(C5=C4C=C(C=C5)O)C)C(=O)OC

Technology Process of Akuammilan-17-oic acid, 1,2-dihydro-10-hydroxy-1-methyl-, methyl ester, (2beta)-

There total 2 articles about Akuammilan-17-oic acid, 1,2-dihydro-10-hydroxy-1-methyl-, methyl ester, (2beta)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-hydroxycathafoline 10-O-α-L-arabinopyranoside → L-(+)-arabinose (87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2) + 10-hydroxycathafoline (81827-54-5)

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 2h;

DOI:10.1080/10286020.2011.649728

Reference yield:

10-hydroxydeformodihydropseudoakuammigine 10-O-α-L-arabinopyranoside → L-(+)-arabinose (87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2) + 10-hydroxycathafoline (81827-54-5)

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 2h;

DOI:10.1080/10286020.2011.649728