Methyl benzoylphosphonochloridate

Base Information

Chemical Name:Methyl benzoylphosphonochloridate
CAS No.:134420-56-7
Molecular Formula:C8H8ClO3P
Molecular Weight:218.576
Hs Code.:
DSSTox Substance ID:DTXSID80564892
Nikkaji Number:J405.045B
Mol file:134420-56-7.mol

Synonyms:Methyl benzoylphosphonochloridate;134420-56-7;DTXSID80564892

Suppliers and Price of Methyl benzoylphosphonochloridate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Methyl benzoylphosphonochloridate

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:217.9899588
Heavy Atom Count:13
Complexity:236

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COP(=O)(C(=O)C1=CC=CC=C1)Cl

Technology Process of Methyl benzoylphosphonochloridate

There total 1 articles about Methyl benzoylphosphonochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117927-83-0
methyl hydrogen benzoylphosphonate

: 134420-56-7
methyl benzoylphosphonochloridate

Guidance literature:: With thionyl chloride; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo00015a040

Reference yield: 87.0%

: 134420-56-7
methyl benzoylphosphonochloridate

: 109-78-4
3-Hydroxypropionitrile

: 159324-43-3
methyl 2-cyanoethyl benzoylphosphonate

Guidance literature:: With pyridine; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

: 134420-56-7
methyl benzoylphosphonochloridate

: Lithium (Z)-1,1,1,3,3,3-hexafluoro-2-propyl (α-hydroxyiminobenzyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: 95 percent / LiBr / acetonitrile / Ambient temperature

3: H₂NOH / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; hydroxylamine; lithium bromide; In dichloromethane; acetonitrile;
DOI:10.1021/jo00079a029